2,6-Dideoxy-3-O-methyl-arabino-hexose

Base Information

• Chemical Name: 2,6-Dideoxy-3-O-methyl-arabino-hexose
• CAS No.: 6786-76-1
• Molecular Formula: C₇H₁₄O₄
• Molecular Weight: 162.186
• UNII: 2X589ALW1D,KYP0P43GXG
• DSSTox Substance ID: DTXSID401044079
• Nikkaji Number: J176.776C
• Mol file: 6786-76-1.mol

Synonyms:2,6-dideoxy-3-O-methyl-arabino-hexose;L-oleandrose;oleandrose

Chemical Property of 2,6-Dideoxy-3-O-methyl-arabino-hexose

Chemical Property:

• Vapor Pressure: 2.68E-05mmHg at 25°C
• Boiling Point: 319.9°Cat760mmHg
• Flash Point: 130.5°C
• PSA: 66.76000
• Density: 1.126g/cm³
• LogP: -0.66790
• XLogP3: -1.3
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 162.08920892
• Heavy Atom Count: 11
• Complexity: 115

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C(C(CC=O)OC)O)O
• Isomeric SMILES: C[C@H]([C@H]([C@@H](CC=O)OC)O)O

Technology Process of 2,6-Dideoxy-3-O-methyl-arabino-hexose

There total 44 articles about 2,6-Dideoxy-3-O-methyl-arabino-hexose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(20S)-12β-acetyloxy, 20-N-methylanthraniloyl 3β,8β,14β,17β-tetrahydroxypregn-6-ene 3-O-β-D-glucopyranosyl-(1→4)-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-β-D-oleandropyranosyl-(1→4)-β-D-cymaropyranosyl-(1→4)-β-D-cymaropyranoside → D-oleandrose (90-56-2,579-04-4,4432-92-2,6786-76-1,13089-76-4,13089-77-5,13484-14-5,22252-39-7,23457-90-1,32791-73-4,85761-09-7,120787-85-1,18607-77-7) + D-symarose (13089-76-4) + D-glucose (50-99-7) + 6-deoxy-3-O-methyl-D-allose (7045-53-6,18546-13-9)

Guidance literature:

With hydrogenchloride; water; In 1,4-dioxane; at 80 ℃; for 3h;

DOI:10.1080/14786419.2019.1663517

Reference yield:

(20S)-12β-acetyloxy, 20-N-methylanthraniloyl 3β,8β,14β,17β-tetrahydroxypregn-6-ene 3-O-β-D-glucopyranosyl-(1→4)-6-deoxy-3-O-methyl-β-D-allopyranosyl-(1→4)-β-D-oleandropyranosyl-(1→4)-β-D-cymaropyranosyl-(1→4)-β-D-cymaropyranosyl-(1→4)-β-D-cymaropyranoside → D-oleandrose (90-56-2,579-04-4,4432-92-2,6786-76-1,13089-76-4,13089-77-5,13484-14-5,22252-39-7,23457-90-1,32791-73-4,85761-09-7,120787-85-1,18607-77-7) + D-symarose (13089-76-4) + D-glucose (50-99-7) + 6-deoxy-3-O-methyl-D-allose (7045-53-6,18546-13-9)

Guidance literature:

With hydrogenchloride; water; In 1,4-dioxane; at 80 ℃; for 3h;

DOI:10.1080/14786419.2019.1663517

Reference yield:

(14S,16S,20R)-14,16-14,20-15,20-triepoxy-14,15-secopregn-5-en-3-ol 3-O-α-L-cymaropyranosyl-(1→4)-β-D-digitoxopyranosyl-(1→4)-β-D-oleandropyranoside → D-digitxose (527-52-6) + D-oleandrose (90-56-2,579-04-4,4432-92-2,6786-76-1,13089-76-4,13089-77-5,13484-14-5,22252-39-7,23457-90-1,32791-73-4,85761-09-7,120787-85-1,18607-77-7) + L-cymarose (32791-73-4)

Guidance literature:

With hydrogenchloride; In methanol; water; at 70 ℃; for 0.25h;

DOI:10.1016/j.cclet.2017.05.017

upstream raw materials:

syriacoside T

Downstream raw materials:

methyl α-D-cymarofuranoside 3,5-dinitrophenylcarbamate

methyl β-D-cymaropyranoside 3,5-dinitrophenylcarbamate

methyl α-D-cymaropyranoside 3,5-dinitrophenylcarbamate

methyl α-L-cymaropyranoside 3,5-dinitrophenylcarbamate

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