tris(cyclohexyloxy)boroxin

Base Information

• Chemical Name: tris(cyclohexyloxy)boroxin
• CAS No.: 1172-69-6
• Molecular Formula: C18H33 B3 O6
• Molecular Weight: 377.889
• Mol file: 1172-69-6.mol

Synonyms:Cyclohexylmetaborate; NSC 149803; Tris(cyclohexyloxy)boroxin

Chemical Property of tris(cyclohexyloxy)boroxin

Chemical Property:

• Vapor Pressure: 4.08E-07mmHg at 25°C
• Boiling Point: 427.4°Cat760mmHg
• Flash Point: 212.3°C
• Density: 1.06g/cm³

Purity/Quality:

98%min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of tris(cyclohexyloxy)boroxin

There total 4 articles about tris(cyclohexyloxy)boroxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

boric acid (11113-50-1,14635-83-7) + cyclohexanol (108-93-0) → tris(cyclohexyloxy)boroxine (1172-69-6)

Guidance literature:

In toluene; byproducts: H2O; boiling; concn., recrystn. from benzene/petroleum ether, elem. anal.;

Reference yield:

cyclohexanol (108-93-0) → tris(cyclohexyloxy)boroxine (1172-69-6)

Guidance literature:

With boric acid; toluene;

DOI:10.1021/ja01611a052

Reference yield:

tricyclohexyl borate (2467-16-5) + boric acid (11113-50-1,14635-83-7) → tris(cyclohexyloxy)boroxine (1172-69-6)

Guidance literature:

excess B(OC6H11)3;;

upstream raw materials:

cyclohexanol

tricyclohexyl borate

boric acid

Downstream raw materials:

cyclohexene

cyclohexane

triisopropylborane