Stannane, trimethyl(2,4,6-trimethylphenyl)-

Base Information

Chemical Name:Stannane, trimethyl(2,4,6-trimethylphenyl)-
CAS No.:1077-62-9
Molecular Formula:C12H20 Sn
Molecular Weight:283.001
Hs Code.:
DSSTox Substance ID:DTXSID5073248
Wikidata:Q82001615
Mol file:1077-62-9.mol

Synonyms:Stannane, trimethyl(2,4,6-trimethylphenyl)-;1077-62-9;Mesityltrimethylstannane;Stannane, mesityltrimethyl-;DTXSID5073248

Suppliers and Price of Stannane, trimethyl(2,4,6-trimethylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, trimethyl(2,4,6-trimethylphenyl)-

Chemical Property:

Vapor Pressure:0.0122mmHg at 25°C
Boiling Point:269.1°C at 760 mmHg
Flash Point:119.1°C
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:284.058703
Heavy Atom Count:13
Complexity:157

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)[Sn](C)(C)C)C

Technology Process of Stannane, trimethyl(2,4,6-trimethylphenyl)-

There total 3 articles about Stannane, trimethyl(2,4,6-trimethylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: [mesitylcopper]5 * toluene

: 1066-45-1
trimethyltin(IV)chloride

: 1077-62-9
SnMe₃(C₆H₂Me₃-2,4,6)

Guidance literature:: In toluene; N2-atmosphere; slow addn. of 1 equiv. (per Cu) Me3SnCl to Cu-compd. at -30°C, slow warming to room temp., stirring for 12 h, heating to 50°C for 1 h; filtration, removal of volatiles (vac.), chromy. (Al2O3, PhMe), evapn. (vac.); elem. anal.;
DOI:10.1021/om9901224

Reference yield: 86.0%

: mesityllithium dimer

: 1066-45-1
trimethyltin(IV)chloride

: 1077-62-9
SnMe₃(C₆H₂Me₃-2,4,6)

Guidance literature:: In hexane; byproducts: LiCl; (inert atm.); addn. of tin compd. to suspn. of lithium compd. in hexane at -20°C, stirring for 1 h at 0°C and then at room temp. for 16 h; filtration, evapn., extn. (pentane) at -78°C, crystn. (pentane) at room temp., elem. anal.;
DOI:10.1039/c0dt00161a