4-Acetylaminomethyl pyridine

Base Information

• Chemical Name: 4-Acetylaminomethyl pyridine
• CAS No.: 23974-15-4
• Molecular Formula: C₈H₁₀N₂O
• Molecular Weight: 150.18
• Hs Code.: 2933399090
• Mol file: 23974-15-4.mol

Synonyms:Acetamide,N-(4-pyridylmethyl)- (8CI); 4-(Acetamidomethyl)pyridine;N-(4-Picolyl)acetamide; N-(4-Pyridylmethyl)acetamide; NSC 152133

Chemical Property of 4-Acetylaminomethyl pyridine

Chemical Property:

• Vapor Pressure: 5.95E-06mmHg at 25°C
• Melting Point: 68-70 °C
• Boiling Point: 379.2°C at 760 mmHg
• PKA: 15.01±0.46(Predicted)
• Flash Point: 183.1°C
• PSA: 41.99000
• Density: 1.088g/cm³
• LogP: 1.10860

Purity/Quality:

98%min ^*data from raw suppliers

N-(Pyridin-4-ylmethyl)acetamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Acetylaminomethyl pyridine

There total 8 articles about 4-Acetylaminomethyl pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

4-(aminomethyl)pyridine (3731-53-1) + benzylidene 1,1-diacetate (581-55-5) → N-(4-Pyridinylmethyl)acetamide (23974-15-4)

Guidance literature:

In neat (no solvent); at 70 ℃; for 16h;

DOI:10.1016/j.tet.2018.05.044

Reference yield: 78.0%

pyridine-4-aldoxime (696-54-8) + acetic acid (64-19-7,77671-22-8) → N-(4-Pyridinylmethyl)acetamide (23974-15-4)

Guidance literature:

With ammonium formate; palladium on activated charcoal; for 0.5h; Heating;

Reference yield: 78.0%

4-(aminomethyl)pyridine (3731-53-1) + 1-acetyl-2,3,4,6,7,8-hexahydropyrrolo[1,2-a]pyrimidinium tetraphenylborate (1363906-80-2) → N-(4-Pyridinylmethyl)acetamide (23974-15-4)

Guidance literature:

In acetonitrile; at 80 ℃; for 1h; Inert atmosphere;

DOI:10.1021/jo202647f

upstream raw materials:

4-(aminomethyl)pyridine

acetic anhydride

acetic acid

pyridine-4-aldoxime

Downstream raw materials:

N-Acetyl-3-(1,1-dimethylethyl)-4-(tetradecyloxy)-N-(4-pyridinylmethyl)benzamide

N-(4-Pyridinylmethyl)-N-[[4-(tetradecyloxy)phenyl]methyl]acetamide

<(1-benzyl-1,2,3,6-tetrahydro-4-pyridyl)methyl>amine

<<1,2,3,6-tetrahydro-1-(4-methoxybenzyl)-4-pyridyl>methyl>amine

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