Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl-

Base Information

• Chemical Name: Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl-
• CAS No.: 1202-62-6
• Molecular Formula: C10H14 N2 O
• Molecular Weight: 178.234
• Hs Code.: 2925290090
• DSSTox Substance ID: DTXSID20903004,DTXSID401238616
• Nikkaji Number: J3.223.287F,J104.397H
• Mol file: 1202-62-6.mol

Synonyms:Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl-;1202-62-6;N'-(4-methoxyphenyl)-N,N-dimethylmethanimidamide;Formamidine, N'-(p-methoxyphenyl)-N,N-dimethyl-;N'-(4-Methoxyphenyl)-N,N-dimethylformamidine;N'-(p-Methoxyphenyl)-N,N-dimethylformamidine;Formamidine, 3,3-dimethyl-1-(4-methoxyphenyl);N'-(4-Methoxyphenyl)-N,N-dimethylimidoformamide #;NoName_3584;NCIOpen2_006829;Oprea1_690604;DTXSID20903004;DTXSID401238616;N-dimethylaminomethylene-p-anisidine;N,N-Dimethyl-N'-(4-methoxyphenyl)formamidine;N/'-(p-Methoxyphenyl)-N,N-dimethylformamidine;4-Methoxy-N-[(E)-(dimethylamino)methylene]aniline

Chemical Property of Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl-

Chemical Property:

• Boiling Point: 274.9oC at 760 mmHg
• Flash Point: 120oC
• PSA: 24.83000
• Density: 0.96g/cm3
• LogP: 1.91660
• XLogP3: 1.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 178.110613074
• Heavy Atom Count: 13
• Complexity: 160

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C=NC1=CC=C(C=C1)OC

Technology Process of Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl-

There total 17 articles about Methanimidamide, N'-(4-methoxyphenyl)-N,N-dimethyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-methoxy-aniline (104-94-9) + N,N-dimethyl-formamide dimethyl acetal (4637-24-5) → N'-(4-methoxyphenyl)-N,N-dimethylformimidamide (1202-62-6)

Guidance literature:

In neat (no solvent); at 80 ℃; Microwave irradiation;

DOI:10.1016/j.tet.2020.131205

Reference yield: 90.0%

4-methoxy-aniline (104-94-9) + 3,5-bis(dimethylaminomethylene)amino-4-nitropyrazole → N'-(4-methoxyphenyl)-N,N-dimethylformimidamide (1202-62-6) + 4-nitro-1H-pyrazole-3,5-diamine (62063-02-9)

Guidance literature:

In methanol; for 4h; Heating;

DOI:10.1023/A:1020921530209

Reference yield: 89.0%

N,N-dimethylformamide diethyl diacetal (1188-33-6) → N'-(4-Methoxy-phenyl)-N,N-dimethyl-formamidine (1202-62-6,56638-70-1)

Guidance literature:

In tetrahydrofuran; at 55 ℃; for 3h;

DOI:10.1002/(SICI)1099-1395(199604)9:4<212::AID-POC775>3.0.CO;2-A

upstream raw materials:

4-methoxy-aniline

N,N-dimethyl-formamide

4-methoxyacetanilide

N,N-dimethylformamide diisopropyl acetal

Downstream raw materials:

3Z-(4-methoxy-anilino)-2-cyano-propenoic acid methyl ester

4-methoxyformanilide

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