2,4-Pentanedione, 3-vanillyl-

Base Information

Chemical Name:2,4-Pentanedione, 3-vanillyl-
CAS No.:30881-23-3
Molecular Formula:C13H16 O4
Molecular Weight:236.268
Hs Code.:
European Community (EC) Number:820-605-0
DSSTox Substance ID:DTXSID80184892
Wikidata:Q83055830
Mol file:30881-23-3.mol

Synonyms:2,4-Pentanedione, 3-vanillyl-;3-Vanillyl-2,4-pentanedione;30881-23-3;2,4-Pentanedione, 3-((4-hydroxy-3-methoxyphenyl)methyl)-;3-(3'-Methoxy-4'-hydroxybenzyl)-2,4-pentandion [German];3-(3'-Methoxy-4'-hydroxybenzyl)-2,4-pentandion;SCHEMBL20721730;DTXSID80184892;LS-101719

Suppliers and Price of 2,4-Pentanedione, 3-vanillyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 26 raw suppliers

Chemical Property of 2,4-Pentanedione, 3-vanillyl-

Chemical Property:

Vapor Pressure:3.55E-06mmHg at 25°C
Boiling Point:375.6°C at 760 mmHg
Flash Point:139.9°C
Density:1.15g/cm³
XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:236.10485899
Heavy Atom Count:17
Complexity:273

Purity/Quality:: 99.9% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C(CC1=CC(=C(C=C1)O)OC)C(=O)C

Technology Process of 2,4-Pentanedione, 3-vanillyl-

There total 4 articles about 2,4-Pentanedione, 3-vanillyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 91418-45-0
3-(4-hydroxy-2-methoxybenzylidene)pentane-2,4-dione

: 30881-23-3
3-(4-hydroxy-3-methoxybenzyl)pentane-2,4-dione

Guidance literature:: With 5%-palladium/activated carbon; hydrogen; In acetone; at 20 ℃; for 1h; under 1034.32 Torr;
DOI:10.2174/1570180811666140512221037

Reference yield:

: 123-54-6,81235-32-7
acetylacetone

: 30881-23-3
3-(4-hydroxy-3-methoxybenzyl)pentane-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 48 h / 20 °C

2: 5%-palladium/activated carbon; hydrogen / acetone / 1 h / 20 °C / 1034.32 Torr

With piperidine; 5%-palladium/activated carbon; hydrogen; In ethanol; acetone; 1: |Knoevenagel Condensation;
DOI:10.2174/1570180811666140512221037

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 30881-23-3
3-(4-hydroxy-3-methoxybenzyl)pentane-2,4-dione

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine / ethanol / 48 h / 20 °C

2: 5%-palladium/activated carbon; hydrogen / acetone / 1 h / 20 °C / 1034.32 Torr

With piperidine; 5%-palladium/activated carbon; hydrogen; In ethanol; acetone; 1: |Knoevenagel Condensation;
DOI:10.2174/1570180811666140512221037