6-Fluoro-1,7-phenanthroline

Base Information

Chemical Name:6-Fluoro-1,7-phenanthroline
CAS No.:191861-16-2
Molecular Formula:C12H7FN2
Molecular Weight:198.1958
Hs Code.:

Synonyms:

Suppliers and Price of 6-Fluoro-1,7-phenanthroline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 6-Fluoro-1,7-phenanthroline

Chemical Property:

Vapor Pressure:2.7E-05mmHg at 25°C
Boiling Point:368.4°C at 760 mmHg
Flash Point:176.6°C
Density:1.336g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-Fluoro-1,7-phenanthroline

There total 4 articles about 6-Fluoro-1,7-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 56-81-5,25618-55-7,64333-26-2,8013-25-0
glycerol

: 175229-87-5
5-amino-8-fluoroquinoline

: 191861-16-2
6-Fluoro-1,7-phenanthroline

Guidance literature:: With sulfuric acid; sodium 3-nitrobenzenesulfonate; at 140 ℃; for 24h;
DOI:10.1248/bpb.20.646

Reference yield:

: 394-68-3
8-fluoroquinoline

: 191861-16-2
6-Fluoro-1,7-phenanthroline

Guidance literature:: Multi-step reaction with 3 steps

1: 60 percent / 61 percent HNO₃; H₂SO₄ / 1 h / 20 °C

2: 65 percent / H₂ / 5 percent Pd/C / benzene

3: 43 percent / sodium m-nitrobenzenesulfonate; 80 percent H₂SO₄ / 24 h / 140 °C

With sulfuric acid; hydrogen; nitric acid; sodium 3-nitrobenzenesulfonate; palladium on activated charcoal; In benzene; 1: Nitration / 2: Reduction / 3: Skraup raction;
DOI:10.1248/bpb.20.646

Reference yield:

: 348-54-9
2-Fluoroaniline

: 191861-16-2
6-Fluoro-1,7-phenanthroline

Guidance literature:: Multi-step reaction with 4 steps

1: sodium m-nitrobenzenesulfonate; 80 percent H₂SO₄ / 4 h / 140 °C

2: 60 percent / 61 percent HNO₃; H₂SO₄ / 1 h / 20 °C

3: 65 percent / H₂ / 5 percent Pd/C / benzene

4: 43 percent / sodium m-nitrobenzenesulfonate; 80 percent H₂SO₄ / 24 h / 140 °C

With sulfuric acid; hydrogen; nitric acid; sodium 3-nitrobenzenesulfonate; palladium on activated charcoal; In benzene; 1: Skraup reaction / 2: Nitration / 3: Reduction / 4: Skraup raction;
DOI:10.1248/bpb.20.646