Ethyl phenethyl carbonate

Base Information

• Chemical Name: Ethyl phenethyl carbonate
• CAS No.: 72928-40-6
• Molecular Formula: C11H14 O3
• Molecular Weight: 194.23
• Hs Code.: 2920909090
• European Community (EC) Number: 277-071-1
• NSC Number: 203411
• DSSTox Substance ID: DTXSID00888320
• Nikkaji Number: J296.407D
• Wikidata: Q82867913
• Mol file: 72928-40-6.mol

Synonyms:Ethyl phenethyl carbonate;72928-40-6;ethyl 2-phenylethyl carbonate;Carbonic acid, ethyl 2-phenylethyl ester;EINECS 277-071-1;Ethyl(phenethyl) carbonate;SCHEMBL2023807;DTXSID00888320;NSC203411;AKOS006243109;NSC 203411;NSC-203411;carbonic acid ethyl 2-phenylethyl ester;A838479

Chemical Property of Ethyl phenethyl carbonate

Chemical Property:

• Vapor Pressure: 0.00652mmHg at 25°C
• Boiling Point: 271.3°C at 760 mmHg
• Flash Point: 102.2°C
• PSA: 35.53000
• Density: 1.069g/cm³
• LogP: 2.40220
• XLogP3: 3.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 194.094294304
• Heavy Atom Count: 14
• Complexity: 162

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)OCCC1=CC=CC=C1

Technology Process of Ethyl phenethyl carbonate

There total 6 articles about Ethyl phenethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-phenylethanol (60-12-8) + Diethyl carbonate (105-58-8,76619-83-5) → ethyl (2-phenyl)ethyl carbonate (72928-40-6)

Guidance literature:

With immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene on magnetic γ-Fe2O3 nanoparticles; at 125 ℃; for 10h;

DOI:10.1002/ejic.201301586

Reference yield: 93.0%

2-phenylethanol (60-12-8) → ethyl (2-phenyl)ethyl carbonate (72928-40-6)

Guidance literature:

With γ-Fe2O3-immobilized 1,5,7-triazabicyclo[4.4.0]dec-5-ene nanoparticles (MNPs-TBD); at 125 ℃; for 10h;

DOI:10.1002/ejic.201301586

Reference yield: 84.0%

ethyl 4,5-dichloro-6-oxopyridazine-1(6H)-carboxylate (17284-90-1) + 2-phenylethanol (60-12-8) → ethyl (2-phenyl)ethyl carbonate (72928-40-6)

Guidance literature:

With aluminum (III) chloride; In toluene; at 20 ℃; for 2h;

DOI:10.5012/bkcs.2014.35.9.2758

upstream raw materials:

2-phenylethanol

chloroformic acid ethyl ester

diethylazodicarboxylate

1-phenyl-2-bromoethane

Downstream raw materials:

styrene