1-(dimethylamino)-3,3-dimethylbutan-2-one

Base Information

Chemical Name:1-(dimethylamino)-3,3-dimethylbutan-2-one
CAS No.:56957-56-3
Molecular Formula:C8H17 N O
Molecular Weight:143.229
Hs Code.:

Synonyms:(Dimethylamino)methyltert-butyl ketone; 1-Dimethylamino-3,3-dimethyl-2-butanone; NSC 234708;tert-Butyl (dimethylamino)methyl ketone

Suppliers and Price of 1-(dimethylamino)-3,3-dimethylbutan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 7 raw suppliers

Chemical Property of 1-(dimethylamino)-3,3-dimethylbutan-2-one

Chemical Property:

Vapor Pressure:1.71mmHg at 25°C
Boiling Point:167.4°Cat760mmHg
Flash Point:43.9°C
Density:0.868g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1-(dimethylamino)-3,3-dimethylbutan-2-one

There total 1 articles about 1-(dimethylamino)-3,3-dimethylbutan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 5469-26-1
1-Bromopinacolon

: 124-40-3
dimethyl amine

: 56957-56-3
1-(dimethylamino)-3,3-dimethylbutan-2-one

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1021/ja204717b

Reference yield: 37.0%

: 56957-56-3
1-(dimethylamino)-3,3-dimethylbutan-2-one

: 368-47-8
phenyltrifluorosilane

: bis[1-(dimethylamino)-3,3-dimethylbut-1-en-2-olato-N,O]fluoro(phenyl)silicon(IV)

Guidance literature:: 1-(dimethylamino)-3,3-dimethylbutan-2-one; With sodium hexamethyldisilazane; In tetrahydrofuran; at 25 ℃; for 2h; Schlenk technique;

phenyltrifluorosilane; In tetrahydrofuran; at 25 ℃; for 20h; Schlenk technique;
DOI:10.1134/S107042801610002X

Reference yield:

: 56957-56-3
1-(dimethylamino)-3,3-dimethylbutan-2-one

: 106625-70-1
ethyl (1-phenylallyl) carbonate

: 79840-73-6,79840-96-3,79840-97-4
4-dimethylamino-2,2-dimethyl-5-phenylhept-6-en-3-one, diastereomer B

: 79840-73-6,79840-96-3,79840-97-4
4-dimethylamino-2,2-dimethyl-5-phenylhept-6-en-3-one, diastereomer A

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; trifuran-2-yl-phosphane; caesium carbonate; In acetonitrile; at 20 ℃; for 4h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ja204717b