(Diethoxymethoxy)benzene

Base Information

• Chemical Name: (Diethoxymethoxy)benzene
• CAS No.: 14444-77-0
• Molecular Formula: C11H16O3
• Molecular Weight: 196.246
• Hs Code.: 2909309090
• European Community (EC) Number: 238-421-9
• UNII: 6WEU8V83SG
• DSSTox Substance ID: DTXSID10162709
• Nikkaji Number: J208.822C
• Wikidata: Q69755193
• Mol file: 14444-77-0.mol

Synonyms:Diethyl phenyl orthoformate;14444-77-0;(Diethoxymethoxy)benzene;Benzene, (diethoxymethoxy)-;diethoxymethoxybenzene;diethoxymethoxy-benzene;DIETHYLPHENYLORTHOFORMATE;EINECS 238-421-9;Orthoformic Acid Diethyl Phenyl Ester;Diethoxyphenoxymethane;phenyl4-aminobenzoate;Diethoxy(phenoxy)methane;(Diethoxymethoxy)benzene #;6WEU8V83SG;DIethylphenYL ORTHOFORMATE;SCHEMBL4865190;DTXSID10162709;MFCD00009228;AKOS015840321;Diethyl phenyl orthoformate, >=97.0%;AS-59097;CS-0320924;FT-0604908;O0187;D91829;J-007951

Chemical Property of (Diethoxymethoxy)benzene

Chemical Property:

• Vapor Pressure: 0.0777mmHg at 25°C
• Melting Point: -26°C
• Refractive Index: n20/D 1.480(lit.)
• Boiling Point: 235.2 °C at 760 mmHg
• Flash Point: 57.2 °C
• PSA: 27.69000
• Density: 1.019 g/cm³
• LogP: 2.42200
• Sensitive.: Moisture Sensitive
• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 196.109944368
• Heavy Atom Count: 14
• Complexity: 127

Purity/Quality:

98%,99%, ^*data from raw suppliers

Diethyl Phenyl Orthoformate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCOC(OCC)OC1=CC=CC=C1

Technology Process of (Diethoxymethoxy)benzene

There total 3 articles about (Diethoxymethoxy)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

orthoformic acid triethyl ester (122-51-0) + phenol (108-95-2,27073-41-2) → diethyl phenyl orthoformate (14444-77-0)

Guidance literature:

With hydrogenchloride; toluene-4-sulfonic acid; In ethanol; under 70 Torr;

Reference yield:

diethoxymethyl acetate (16326-34-4) + phenol (108-95-2,27073-41-2) → diethyl phenyl orthoformate (14444-77-0)

Guidance literature:

Reference yield:

→ diethyl phenyl orthoformate (14444-77-0)

Guidance literature:

upstream raw materials:

orthoformic acid triethyl ester

phenol

diethoxymethyl acetate

Downstream raw materials:

7,7-diethoxy-hept-3c-ene

cyclohexa-2,5-dienylethanal diethylacetal

1.1-Diethoxy-4-dimethylaminobutin-(2)

phenylpropionaldehyde diethyl acetal