2,4-DICHLOROBENZYL MERCAPTAN

Base Information

• Chemical Name: 2,4-DICHLOROBENZYL MERCAPTAN
• CAS No.: 65909-82-2
• Molecular Formula: C7H6Cl2S
• Molecular Weight: 193.09
• Mol file: 65909-82-2.mol

Synonyms:2.4-Dichlor-thioanisol;2,4-dichloro-1-methylsulfanyl-benzene;2,4-dichloro-1-methylthiobenzene;2,4-Dichlorothioanisole;

Chemical Property of 2,4-DICHLOROBENZYL MERCAPTAN

Chemical Property:

• Vapor Pressure: 0.0491mmHg at 25°C
• Boiling Point: 115 °C / 2mmHg
• Flash Point: 101°C
• PSA: 25.30000
• Density: 1.36
• LogP: 3.71530

Purity/Quality:

99% ^*data from raw suppliers

(2,4-Dichlorophenyl)(methyl)sulfane 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-DICHLOROBENZYL MERCAPTAN

There total 4 articles about 2,4-DICHLOROBENZYL MERCAPTAN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

Dimethyldisulphide (624-92-0) + 2,4-Dichloroaniline (554-00-7,51908-09-9) → 2,4-dichloro-1-methylthiobenzene (65909-82-2)

Guidance literature:

With isopentyl nitrite; In acetonitrile; Heating;

DOI:10.1081/SCC-100104335

Reference yield:

→ 2,4-dichloro-1-methylthiobenzene (65909-82-2)

Guidance literature:

With copper(l) chloride; at 60 - 70 ℃;

Reference yield:

2,4-dichloro-benzenethiol; sodium salt (61713-34-6) + methyl iodide (74-88-4) → 2,4-dichloro-1-methylthiobenzene (65909-82-2)

Guidance literature:

With ethanol;

upstream raw materials:

2,4-dichloro-benzenethiol; sodium salt

methyl iodide

Dimethyldisulphide

2,4-Dichloroaniline

Downstream raw materials:

2,4-dichloro-methylsulfonylbenzene

(2,4-dichloro-phenyl)-trichloromethyl sulfide

2,4-dichloro-methylsulfinylbenzene