Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester

Base Information

Chemical Name:Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester
CAS No.:61222-49-9
Molecular Formula:C₁₅H₂₅O₄P
Molecular Weight:300.335
Hs Code.:
DSSTox Substance ID:DTXSID80886425
Nikkaji Number:J1.607.848D

Synonyms:dibutoxyphosphoryl(phenyl)methanol;61222-49-9;Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester;Dibutyl (alpha-hydroxybenzyl)phosphonate;Phosphonic acid, (hydroxyphenylmethyl)-, dibutyl ester;DTXSID80886425;STK722123;AKOS005524127;dibutyl [hydroxy(phenyl)methyl]phosphonate;(Hydroxyphenylmethyl)phosphonic acid dibutyl ester

Suppliers and Price of Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester

Chemical Property:

Vapor Pressure:1.17E-07mmHg at 25°C
Boiling Point:415.8°C at 760 mmHg
Flash Point:205.3°C
Density:1.1g/cm³
XLogP3:2.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:10
Exact Mass:300.14904627
Heavy Atom Count:20
Complexity:276

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCOP(=O)(C(C1=CC=CC=C1)O)OCCCC

Technology Process of Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester

There total 3 articles about Phosphonic acid, P-(hydroxyphenylmethyl)-, dibutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-52-7
benzaldehyde

: 109-73-9,85404-21-3
N-butylamine

: 762-04-9
phosphonic acid diethyl ester

: dibutyl ((butylamino)(phenyl)methyl)phosphonate

: 61222-49-9
dibutyl hydroxy(phenyl)methylphosphonate

Guidance literature:: In ethanol; at 120 ℃; for 0.5h; under 12929 Torr; Microwave irradiation; Flow reactor;
DOI:10.1080/10426507.2018.1528253

Reference yield:

: 1809-19-4
dibutyl hydrogen phosphite

: 100-52-7
benzaldehyde

: 61222-49-9
dibutyl hydroxy(phenyl)methylphosphonate

Guidance literature:: With sodium methylate;

Reference yield:

: 102-85-2
tri-n-butyl phosphite

: 61222-49-9
dibutyl hydroxy(phenyl)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: water / tetrahydrofuran / 12 h / Inert atmosphere; Reflux

2.1: triethylamine; iron(III) chloride / tetrahydrofuran / 0.25 h

2.2: 24 h

With iron(III) chloride; water; triethylamine; In tetrahydrofuran;
DOI:10.1002/adsc.201300653