2-CHLORO-N-(2-PHENYLETHYL)PROPANAMIDE

Base Information

• Chemical Name: 2-CHLORO-N-(2-PHENYLETHYL)PROPANAMIDE
• CAS No.: 13156-97-3
• Molecular Formula: C11H14 Cl N O
• Molecular Weight: 211.691
• Hs Code.: 2924299090
• Mol file: 13156-97-3.mol

Synonyms:Propionamide,2-chloro-N-phenethyl- (6CI,8CI)

Chemical Property of 2-CHLORO-N-(2-PHENYLETHYL)PROPANAMIDE

Chemical Property:

• Vapor Pressure: 5.19E-06mmHg at 25°C
• Boiling Point: 381.1°C at 760 mmHg
• Flash Point: 184.3°C
• PSA: 32.59000
• Density: 1.117g/cm³
• LogP: 2.81290

Purity/Quality:

97% ^*data from raw suppliers

2-chloro-N-(2-phenylethyl)propanamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-CHLORO-N-(2-PHENYLETHYL)PROPANAMIDE

There total 2 articles about 2-CHLORO-N-(2-PHENYLETHYL)PROPANAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

2-chloropropionyl chloride (7623-09-8) + phenethylamine (64-04-0) → 2-chloro-N-phenylethylpropanamide (13156-97-3)

Guidance literature:

With potassium carbonate; In dichloromethane; Heating;

DOI:10.1081/SCC-120030689

Reference yield:

→ 2-chloro-N-phenylethylpropanamide (13156-97-3)

Guidance literature:

/BRN= 3437909/;

DOI:10.1021/ja01604a047

Reference yield: 96.0%

2-chloro-3-hydroxypyridine (6636-78-8) + 2-chloro-N-phenylethylpropanamide (13156-97-3) → 2-(2-chloropyridin-3-yloxy)-N-phenethylpropionamide (596808-12-7)

Guidance literature:

With potassium carbonate; In acetonitrile; Heating;

DOI:10.1021/jo034593i

upstream raw materials:

2-chloropropionyl chloride

phenethylamine

Downstream raw materials:

2-(2-chloropyridin-3-yloxy)-N-phenethylpropionamide

1,2,4,5-tetrahydro-3-methyl-3H-3-benzazepin-2-one

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