N'-(2-Nitrophenyl)acetohydrazide

Base Information

• Chemical Name: N'-(2-Nitrophenyl)acetohydrazide
• CAS No.: 14674-17-0
• Molecular Formula: C8H9 N3 O3
• Molecular Weight: 195.178
• DSSTox Substance ID: DTXSID20163469
• Nikkaji Number: J86.258D
• Wikidata: Q83032360
• Mol file: 14674-17-0.mol

Synonyms:N'-(2-Nitrophenyl)acetohydrazide;14674-17-0;ACETIC ACID, 2-(o-NITROPHENYL)HYDRAZIDE;BRN 1842502;2-(o-Nitrophenyl)acetyl hydrazide;4-15-00-00310 (Beilstein Handbook Reference);2-Acethydrazidonitrobenzene;DTXSID20163469;N'-(o-Nitrophenyl)acetohydrazide;YEMZEMNLHVJVJK-UHFFFAOYSA-N;N/'-(2-Nitrophenyl)acetohydrazide;N'-(2-Nitrophenyl)acetohydrazide #;AKOS006242250;ACETIC ACID N'-(2-NITRO-PHENYL)-HYDRAZIDE

Chemical Property of N'-(2-Nitrophenyl)acetohydrazide

Chemical Property:

• Vapor Pressure: 0.00159mmHg at 25°C
• Boiling Point: 294.8°C at 760 mmHg
• Flash Point: 132.1°C
• PSA: 90.44000
• Density: 1.363g/cm³
• LogP: 2.49430
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 195.06439116
• Heavy Atom Count: 14
• Complexity: 226

Purity/Quality:

99% ^*data from raw suppliers

N'-(2-Nitrophenyl)acetohydrazide 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)NNC1=CC=CC=C1[N+](=O)[O-]

Technology Process of N'-(2-Nitrophenyl)acetohydrazide

There total 8 articles about N'-(2-Nitrophenyl)acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

acetic anhydride (108-24-7) + (2-nitrophenyl)hydrazine (3034-19-3) → acetic acid 2-(2-nitrophenyl)hydrazide (14674-17-0)

Guidance literature:

Reference yield: 11.0%

acetic acid hydrazide (1068-57-1) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → acetic acid 2-(2-nitrophenyl)hydrazide (14674-17-0)

Guidance literature:

In 2-methoxy-ethanol; for 5.5h; Heating;

DOI:10.1021/jm00131a010

Reference yield:

sodium acetate (127-09-3) + (2-nitrophenyl)hydrazine (3034-19-3) → acetic acid 2-(2-nitrophenyl)hydrazide (14674-17-0)

Guidance literature:

In acetic acid; at 95 ℃; for 1h;

upstream raw materials:

Ketene

(2-nitrophenyl)hydrazine

N-acetylacetamide

acetic anhydride

Downstream raw materials:

N,N'-diacetyl-N-(2-nitro-phenyl)-hydrazine

3-methylbenzo[e][1,2,4]triazine

1-amino-2-methylbenzimidazole

1-acetamido-2-benzimidazolinone