n,n-Dimethyl-9h-fluoren-9-amine

Base Information

• Chemical Name: n,n-Dimethyl-9h-fluoren-9-amine
• CAS No.: 53156-46-0
• Molecular Formula: C15H15N
• Molecular Weight: 209.291
• Hs Code.: 2921499090
• NSC Number: 100810
• DSSTox Substance ID: DTXSID60295258
• Nikkaji Number: J484.621D
• Wikidata: Q82035083
• Mol file: 53156-46-0.mol

Synonyms:n,n-dimethyl-9h-fluoren-9-amine;53156-46-0;NSC100810;NCIOpen2_006767;SCHEMBL1509312;DTXSID60295258;AKOS024337464;NSC-100810

Chemical Property of n,n-Dimethyl-9h-fluoren-9-amine

Chemical Property:

• Vapor Pressure: 0.000111mmHg at 25°C
• Boiling Point: 336.6°C at 760 mmHg
• Flash Point: 142.7°C
• PSA: 3.24000
• Density: 1.11g/cm³
• LogP: 3.31800
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 1
• Exact Mass: 209.120449483
• Heavy Atom Count: 16
• Complexity: 226

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

9-(DIMETHYLAMINO)FLUORENE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1C2=CC=CC=C2C3=CC=CC=C13

Technology Process of n,n-Dimethyl-9h-fluoren-9-amine

There total 3 articles about n,n-Dimethyl-9h-fluoren-9-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 9H-fluoren-9-yl bromide (1940-57-4) → 9-fluorenone (486-25-9,952573-42-1) + 9-Fluorenol (1689-64-1) + 9-(N,N-dimethylamino)fluorene (53156-46-0)

Guidance literature:

at 155 - 160 ℃;

DOI:10.1039/b211792d

Reference yield:

9H-fluoren-9-yl bromide (1940-57-4) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 9-fluorenone (486-25-9,952573-42-1) + 9-Fluorenol (1689-64-1) + 9-(N,N-dimethylamino)fluorene (53156-46-0)

Guidance literature:

at 155 - 160 ℃;

DOI:10.1039/b211792d

Reference yield:

N-(9-fluorenyl)trimethylammonium bromide (6634-60-2) → tetrabenzo[5.5]fulvalene (746-47-4) + 9-(N,N-dimethylamino)fluorene (53156-46-0) + di-fluoren-9-yl ether (31859-93-5) + trimethylamine (75-50-3)

Guidance literature:

Erhitzes der erhaltene frei Base;

upstream raw materials:

N-(9-fluorenyl)trimethylammonium bromide

N,N,N,N,N,N-hexamethylphosphoric triamide

9H-fluoren-9-yl bromide

N,N-dimethyl-formamide

Downstream raw materials:

2-(9-fluorenylidene)-1-phenylethanone

2,5-dimethylhexane

1,2-bis(phenylsulfonyl)ethane

2,6-dimethylphenylmethyl-9-fluorenyldimethylammonium bromide

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