3-(2-hydroxy-1-naphthyl)propanenitrile

Base Information

• Chemical Name: 3-(2-hydroxy-1-naphthyl)propanenitrile
• CAS No.: 14233-73-9
• Molecular Formula: C13H11NO
• Molecular Weight: 197.23254
• Hs Code.: 2926909090
• Mol file: 14233-73-9.mol

Synonyms:1-Naphthalenepropionitrile,2-hydroxy- (6CI,7CI,8CI);1-(2-Cyanoethyl)-2-hydroxynaphthalene;1-(2-Cyanoethyl)-2-naphthol;NSC 6904;

Chemical Property of 3-(2-hydroxy-1-naphthyl)propanenitrile

Chemical Property:

• Vapor Pressure: 4.77E-08mmHg at 25°C
• Refractive Index: 1.65
• Boiling Point: 431.4 °C at 760 mmHg
• Flash Point: 214.7 °C
• PSA: 44.02000
• Density: 1.197 g/cm³
• LogP: 3.00158

Purity/Quality:

98% ^*data from raw suppliers

3-(2-Hydroxy-1-naphthyl)propanenitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-hydroxy-1-naphthyl)propanenitrile

There total 7 articles about 3-(2-hydroxy-1-naphthyl)propanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

endo-4-cyanotricyclo<6.4.0.02,5>dodeca-1(12),6,8,10-tetraen-5-ol (76466-81-4) → 3-(2-hydroxynaphthalen-1-yl)propanenitrile (14233-73-9)

Guidance literature:

With sodium hydroxide; at 20 ℃; for 12h;

DOI:10.1021/jo00320a041

Reference yield: 76.0%

7-cyano-2,3-benzobicyclo<4.2.0>octa-2,4-dien-6-ol trimethylsilyl ether (76466-82-5) → 3-(2-hydroxynaphthalen-1-yl)propanenitrile (14233-73-9)

Guidance literature:

With sodium hydroxide; at 20 ℃; for 12h;

DOI:10.1021/jo00320a041

Reference yield: 43.0%

acrylonitrile (107-13-1,25014-41-9) + β-naphthol (135-19-3) → 3-(2-hydroxynaphthalen-1-yl)propanenitrile (14233-73-9)

Guidance literature:

acrylonitrile; β-naphthol; With sodium hydroxide; In benzene; for 3h; Reflux;

With hydrogenchloride; water; pH=2;

DOI:10.1016/j.tetlet.2010.06.128

upstream raw materials:

tetrachloromethane

acrylonitrile

β-naphthol

benzene

Downstream raw materials:

3-(2-phenylnaphthalen-1-yl)propanoic acid

ethyl 3-(2-phenylnaphthalen-1-yl)propanoate

4-(4-fluorophenyl)-1H-phenalen-1-one

4-(4-fluorophenyl)-2,3-dihydro-1H-phenalen-1-one

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