1-(p-Chlorobenzoyl)-2-isopropylhydrazine

Base Information

Chemical Name:1-(p-Chlorobenzoyl)-2-isopropylhydrazine
CAS No.:19436-42-1
Molecular Formula:C10H13ClN2O
Molecular Weight:212.679
Hs Code.:2928000090
NSC Number:522515,169907
UNII:23AQR42WXV
DSSTox Substance ID:DTXSID20941168
Nikkaji Number:J49.476C
Wikidata:Q82917956
ChEMBL ID:CHEMBL3277566
Mol file:19436-42-1.mol

Synonyms:19436-42-1;1-(p-Chlorobenzoyl)-2-isopropylhydrazine;4-chloro-N'-propan-2-ylbenzohydrazide;Hydrazine, 1-(p-chlorobenzoyl)-2-isopropyl-;Benzoic acid, p-chloro-, 2-isopropylhydrazide;23AQR42WXV;Benzoic acid, 4-chloro-, 2-(1-methylethyl)hydrazide;1-(4-Chlorobenzoyl)-2-(1-methylethyl)hydrazine;NSC-169907;NSC-522515;4-chloro-n'-isopropylbenzohydrazide;NSC 169907;Ro 4-1027;BRN 2578727;NSC169907;UNII-23AQR42WXV;CHEMBL3277566;SCHEMBL15486113;DTXSID20941168;QHZLYJFTHWJCAB-UHFFFAOYSA-N;NSC522515;4-Chloro-N'-(propan-2-yl)benzohydrazide;4-Chlorobenzoic acid 2-(1-methylethyl)hydrazide

Suppliers and Price of 1-(p-Chlorobenzoyl)-2-isopropylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(p-Chlorobenzoyl)-2-isopropylhydrazine

Chemical Property:

Boiling Point:288.4oC at 760 mmHg
Flash Point:128.2oC
PSA：41.13000
Density:1.156g/cm3
LogP:2.76460
XLogP3:2.4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:212.0716407
Heavy Atom Count:14
Complexity:189

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)NNC(=O)C1=CC=C(C=C1)Cl

Technology Process of 1-(p-Chlorobenzoyl)-2-isopropylhydrazine

There total 2 articles about 1-(p-Chlorobenzoyl)-2-isopropylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 86512-60-9
acetone-N-(4-chlorobenzoyl)hydrazone

: 19436-42-1
4-chloro-N'-isopropylbenzohydrazide

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 18h;
DOI:10.1055/s-2005-869858

Reference yield:

: 536-40-3
4-chlorobenzoic acid hydrazide

: 19436-42-1
4-chloro-N'-isopropylbenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / Na₂SO₄ / 18 h / 20 °C

2: 91 percent / NaCNBH₃; AcOH / methanol / 18 h / 20 °C

With sodium cyanoborohydride; acetic acid; sodium sulfate; In methanol;
DOI:10.1055/s-2005-869858

Reference yield: 49.0%

: 19436-42-1
4-chloro-N'-isopropylbenzohydrazide

: 359700-09-7
(E)-3-(1-(tert-butoxycarbonyl)-1H-indol-3-yl)acrylic acid

: 1407499-52-8
(E)-tert-butyl 3-(3-(2-(4-chlorobenzoyl)-1-isopropylhydrazinyl)-3-oxoprop-1-enyl)-1H-indole-1-carboxylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 12h;