N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester

Base Information

Chemical Name:N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester
CAS No.:2231-31-4
Molecular Formula:C₇H₁₆NO₅P
Molecular Weight:225.181
Hs Code.:
Mol file:2231-31-4.mol

Synonyms:Carbamicacid, methylphosphono-, C-isopropyl P,P-dimethyl ester (7CI); Carbamic acid, methylphosphono-,C-isopropyl dimethyl ester (8CI); Demuphos; DimethylN-methylisopropylurethanephosphate

Suppliers and Price of N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester

Chemical Property:

Boiling Point:73 - 77 °C (0.07 mmHg)
PSA：74.88000
LogP:1.86410

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester

There total 6 articles about N-(Dimethoxyphosphinyl)-N-methylcarbamic acid 1-methylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 67-56-1
methanol

: 70746-00-8
(isopropoxycarbonyl)methylphosphoramidic dichloride

: 2231-31-4
dimethyl (isopropoxycarbonyl)methylphosphoramidate

Guidance literature:: With triethylamine; In diethyl ether; for 2h;

Reference yield:

: 15586-26-2
isopropyl chloromethylcarbamate

: 2231-31-4
dimethyl (isopropoxycarbonyl)methylphosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1: 50 percent / methyl phosphorodichloridite / anhydrous ferric chloride / benzene / Heating; 1.5-2 h

2: 73 percent / triethylamine / diethyl ether / 2 h

With methyl dichlorophosphite; triethylamine; iron(III) chloride; In diethyl ether; benzene;