2-(Acetyloxymethoxy)ethoxymethyl acetate

Base Information

• Chemical Name: 2-(Acetyloxymethoxy)ethoxymethyl acetate
• CAS No.: 90114-17-3
• Molecular Formula: C8H14O6
• Molecular Weight: 206.196
• NSC Number: 57560
• DSSTox Substance ID: DTXSID90288774
• Wikidata: Q82025865
• Mol file: 90114-17-3.mol

Synonyms:90114-17-3;2-(acetyloxymethoxy)ethoxymethyl acetate;ethane-1,2-diylbis(oxymethanediyl) diacetate;(Ethane-1,2-diylbis(oxy))bis(methylene) diacetate;NSC57560;starbld0003163;SCHEMBL3392872;DTXSID90288774;NSC-57560

Chemical Property of 2-(Acetyloxymethoxy)ethoxymethyl acetate

Chemical Property:

• Vapor Pressure: 0.0173mmHg at 25°C
• Refractive Index: 1.425
• Boiling Point: 254.36 °C at 760 mmHg
• Flash Point: 105.564 °C
• PSA: 71.06000
• Density: 1.144 g/cm³
• LogP: 0.06080
• XLogP3: -0.1
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 9
• Exact Mass: 206.07903816
• Heavy Atom Count: 14
• Complexity: 159

Purity/Quality:

99% ^*data from raw suppliers

1,2-Bis(acetoxy-methyloxy)ethane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)OCOCCOCOC(=O)C
• Uses: 1,2-Bis(acetoxy-methyloxy)ethane is synthesized from 1,2-Ethylene glycol (E890140), which is used in the production of nanocables and nanotubes.

Technology Process of 2-(Acetyloxymethoxy)ethoxymethyl acetate

There total 3 articles about 2-(Acetyloxymethoxy)ethoxymethyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

1,2-bis(chloromethoxy)ethane (13483-18-6) + sodium acetate (127-09-3) → 1,2-bis(acetoxy-methyloxy)ethane (90114-17-3)

Guidance literature:

at 90 ℃; for 2.5h; Cooling with ice;

DOI:10.3390/molecules17088735

Reference yield:

1,3-DIOXOLANE (646-06-0) + sulfuric acid (7664-93-9) + sodium acetate (127-09-3) + acetic anhydride (108-24-7) → ethylene glycol diacetate (111-55-7,27252-83-1) + 2-acetoxyethyl acetoxymethyl ether (59278-00-1) + 1,2-bis(acetoxy-methyloxy)ethane (90114-17-3)

Guidance literature:

Reference yield:

1,3-DIOXOLANE (646-06-0) + acetic anhydride (108-24-7) → 1,2-bis(acetoxy-methyloxy)ethane (90114-17-3)

Guidance literature:

With sulfuric acid; Versetzen des abgekuehlten Reaktionsgemisches mit Natriumacetat_.;

upstream raw materials:

1,2-bis(chloromethoxy)ethane

sodium acetate

1,3-DIOXOLANE

sulfuric acid

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