1-Phenyl-2-pyridin-4-ylethane-1,2-dione

Base Information

Chemical Name:1-Phenyl-2-pyridin-4-ylethane-1,2-dione
CAS No.:35779-40-9
Molecular Formula:C13H9NO2
Molecular Weight:211.22
Hs Code.:
NSC Number:121399
DSSTox Substance ID:DTXSID60957167
Nikkaji Number:J2.176.850B
Wikidata:Q82937401
Mol file:35779-40-9.mol

Synonyms:35779-40-9;1-phenyl-2-pyridin-4-ylethane-1,2-dione;1-phenyl-2-(pyridin-4-yl)ethane-1,2-dione;NSC121399;SCHEMBL3074392;DTXSID60957167;LXHDDNZEFUEFDI-UHFFFAOYSA-N;1 -phenyl-2-(4-pyridinyl)ethanedione;NSC-121399;FT-0759465

Suppliers and Price of 1-Phenyl-2-pyridin-4-ylethane-1,2-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-Phenyl-2-pyridin-4-ylethane-1,2-dione

Chemical Property:

Vapor Pressure:9.72E-06mmHg at 25°C
Boiling Point:372.3°C at 760 mmHg
Flash Point:182.4°C
Density:1.216g/cm³
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:211.063328530
Heavy Atom Count:16
Complexity:263

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)C(=O)C2=CC=NC=C2

Technology Process of 1-Phenyl-2-pyridin-4-ylethane-1,2-dione

There total 10 articles about 1-Phenyl-2-pyridin-4-ylethane-1,2-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 35779-40-9
1-phenyl-2-(pyridin-4-yl)ethane-1,2-dione

Guidance literature:

Reference yield: 64.0%

: 13295-94-8
4-(phenylethynyl)pyridine

: 35779-40-9
1-phenyl-2-(pyridin-4-yl)ethane-1,2-dione

Guidance literature:: With potassium permanganate; magnesium sulfate heptahydrate; sodium hydrogencarbonate; In water; acetone; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acscombsci.5b00107

Reference yield: 26.0%

: 2510-22-7
4-pyridylacetylene

: 591-50-4
iodobenzene

: 35779-40-9
1-phenyl-2-(pyridin-4-yl)ethane-1,2-dione

Guidance literature:: 4-pyridylacetylene; iodobenzene; With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; In dimethyl sulfoxide; at 50 ℃; for 4h; Schlenk technique; Inert atmosphere;

With oxygen; at 150 ℃; for 20h; Temperature; Schlenk technique;
DOI:10.1002/ejoc.201900783