2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester

Base Information

Chemical Name:2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester
CAS No.:102233-68-1
Molecular Formula:C11H15NO2S
Molecular Weight:225.312
Hs Code.:
Mol file:102233-68-1.mol

Synonyms:2-Butenoic acid,3-[[2-(3-thienyl)ethyl]amino]-,methyl ester;methyl 3-crotonate;

Suppliers and Price of 2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester

Chemical Property:

PSA：66.57000
LogP:2.34790

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester

There total 1 articles about 2-Butenoic acid, 3-[[2-(3-thienyl)ethyl]amino]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 59311-67-0
2-(3-thienyl)ethylamine

: 105-45-3
acetoacetic acid methyl ester

: 102233-68-1
methyl 3-crotonate

Guidance literature:: Ambient temperature;
DOI:10.1021/jo00362a008

Reference yield:

: 59311-67-0
2-(3-thienyl)ethylamine

: 100-52-7
benzaldehyde

: 102233-68-1
methyl 3-crotonate

: dimethyl 2,6-dimethyl-4-phenyl-N-<2-(3-thienyl)ethyl>-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: With titanium tetrachloride; Yield given. Multistep reaction; 1.) benzene, 2.) benzene, RT, 24 h;
DOI:10.1021/jo00362a008

Reference yield:

: 102233-68-1
methyl 3-crotonate

: dimethyl 4,9,10,10a-tetrahydro-7,10aα-dimethyl-9β-phenyl-5H-thieno<2,3-a>quinolizine-8,10β-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) TiCl₄ / 1.) benzene, 2.) benzene, RT, 24 h

2: TiCl₄ / CHCl₃ / 24 h / Ambient temperature

With titanium tetrachloride; In chloroform;
DOI:10.1021/jo00362a008