2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester

Base Information

Chemical Name:2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester
CAS No.:104387-18-0
Molecular Formula:C18H16O4
Molecular Weight:296.323
Hs Code.:
DSSTox Substance ID:DTXSID60358756
Mol file:104387-18-0.mol

Synonyms:2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester;104387-18-0;DTXSID60358756

Suppliers and Price of 2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester

Chemical Property:

XLogP3:3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:296.10485899
Heavy Atom Count:22
Complexity:407

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)C1=CC=CC=C1OC(=O)C=CC2=CC=C(C=C2)OC

Technology Process of 2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester

There total 3 articles about 2-Propenoic acid, 3-(4-methoxyphenyl)-, 2-acetylphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 830-09-1
3-(4'-methoxyphenyl)propenoic acid

: 104387-18-0
(E)-3-(4-Methoxy-phenyl)-acrylic acid 2-acetyl-phenyl ester

Guidance literature:: With pyridine; trichlorophosphate; at 60 ℃;
DOI:10.1016/j.bmc.2010.05.006

Reference yield:

: 118-93-4,104809-67-8
o-hydroxyacetophenone

: 42996-84-9,34446-64-5
p-methoxycinnamoyl chloride

: 104387-18-0
(E)-3-(4-Methoxy-phenyl)-acrylic acid 2-acetyl-phenyl ester

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1016/j.bmc.2010.07.044

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 104387-18-0
(E)-3-(4-Methoxy-phenyl)-acrylic acid 2-acetyl-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine; piperidine / 6 h / Reflux

2: pyridine; trichlorophosphate / 20 °C / Cooling with ice

With piperidine; pyridine; trichlorophosphate; 1: |Knoevenagel Condensation;
DOI:10.3390/molecules191016058