[2-(Cyclohex-1-en-1-yl)ethyl]benzene

Base Information

• Chemical Name: [2-(Cyclohex-1-en-1-yl)ethyl]benzene
• CAS No.: 15232-90-3
• Molecular Formula: C14H18
• Molecular Weight: 186.297
• Hs Code.: 2902909090
• NSC Number: 28067
• DSSTox Substance ID: DTXSID20282806
• Wikidata: Q82017171
• Mol file: 15232-90-3.mol

Synonyms:2-(cyclohexen-1-yl)ethylbenzene;[2-(cyclohex-1-en-1-yl)ethyl]benzene;15232-90-3;NSC28067;DTXSID20282806;1-cyclohexen-1-yl-2-phenylethane;1-(1-cyclohexenyl)-2-phenylethane;NSC-28067;AKOS006316909;2-(1-CYCLOHEXENYL)ETHYLBENZENE

Chemical Property of [2-(Cyclohex-1-en-1-yl)ethyl]benzene

Chemical Property:

• Vapor Pressure: 0.00505mmHg at 25°C
• Boiling Point: 284.7°Cat760mmHg
• Flash Point: 122.7°C
• PSA: 0.00000
• Density: 0.95g/cm³
• LogP: 4.11960
• XLogP3: 4.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 3
• Exact Mass: 186.140850574
• Heavy Atom Count: 14
• Complexity: 184

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC(=CC1)CCC2=CC=CC=C2

Technology Process of [2-(Cyclohex-1-en-1-yl)ethyl]benzene

There total 19 articles about [2-(Cyclohex-1-en-1-yl)ethyl]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-phenethyl-2-(phenylsulfonyl)-1-thiacycloheptane S,S-dioxide (130220-18-7) → (2-(cyclohex-1-en-1-yl)ethyl)benzene (15232-90-3)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; for 0.0833333h;

Reference yield:

1-phenethyl-cyclohexanol (124620-30-0) → (2-(cyclohex-1-en-1-yl)ethyl)benzene (15232-90-3)

Guidance literature:

With iodine; Destillation;

DOI:10.1021/jo01232a008

Reference yield:

1-Methyl-4-(3-phenethyl-cyclohex-2-enesulfonyl)-benzene (109951-10-2) → (2-(cyclohex-1-en-1-yl)ethyl)benzene (15232-90-3)

Guidance literature:

With lithium triethylborohydride; bis(diphenylphosphino)propanepalladium(II) dichloride; In tetrahydrofuran; at 0 ℃; for 0.5h; Yield given;

DOI:10.1246/cl.1986.1177

upstream raw materials:

2-(cyclohex-1-en-1-yl)-1-phenylethan-1-one

1-phenethyl-cyclohexanol

2-phenethyl-2-(phenylsulfonyl)-1-thiacycloheptane S,S-dioxide

1-Methyl-4-(3-phenethyl-cyclohex-2-enesulfonyl)-benzene

Downstream raw materials:

1,2-epoxy-1-phenethyl-cyclohexane

(E)-1,2-diphenyl-ethene

anti-1,2-dibromo-1,2-diphenylethane

6-oxo-8-phenyloctanal