1-(4-Methylphenyl)-6-phenylhexane-1,6-dione

Base Information

Chemical Name:1-(4-Methylphenyl)-6-phenylhexane-1,6-dione
CAS No.:106696-59-7
Molecular Formula:C19H20O2
Molecular Weight:280.367
Hs Code.:
DSSTox Substance ID:DTXSID30544705
Wikidata:Q82421929

Synonyms:106696-59-7;1-(4-Methylphenyl)-6-phenylhexane-1,6-dione;DTXSID30544705

Suppliers and Price of 1-(4-Methylphenyl)-6-phenylhexane-1,6-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-Methylphenyl)-6-phenylhexane-1,6-dione

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:280.146329876
Heavy Atom Count:21
Complexity:334

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)CCCCC(=O)C2=CC=CC=C2

Technology Process of 1-(4-Methylphenyl)-6-phenylhexane-1,6-dione

There total 7 articles about 1-(4-Methylphenyl)-6-phenylhexane-1,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 106696-60-0
5-(p-toluoyl)valeroyl chloride

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 106696-59-7
1-phenyl-6-(p-tolyl)hexane-1,6-dione

Guidance literature:: With aluminium trichloride; for 2h; Ambient temperature;
DOI:10.1246/bcsj.59.1087

Reference yield: 35.0%

: 40122-37-0
1-(p-tolyl)cyclopropan-1-ol

: 768-03-6,26742-84-7
Phenyl vinyl ketone

: 106696-59-7
1-phenyl-6-(p-tolyl)hexane-1,6-dione

Guidance literature:: With manganous acetylacetonate; at 120 ℃; for 8h; Sealed tube; Green chemistry;
DOI:10.1021/acs.orglett.9b01703

Reference yield:

: 100-52-7
benzaldehyde

: 106696-59-7
1-phenyl-6-(p-tolyl)hexane-1,6-dione

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether; tetrahydrofuran / 4 h / -20 °C

2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 2 h / 20 °C

3: manganous acetylacetonate / 8 h / 120 °C / Sealed tube; Green chemistry

With manganous acetylacetonate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1021/acs.orglett.9b01703