Cyclopropanecarboxylic acid, 3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethyl-, (2-methyl[1,1'-biphenyl]-3-yl)methyl ester

Base Information

• Chemical Name: Cyclopropanecarboxylic acid, 3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethyl-, (2-methyl[1,1'-biphenyl]-3-yl)methyl ester
• CAS No.: 110171-52-3
• Molecular Formula: C23H23Cl2F3O3
• Molecular Weight: 475.335
• Mol file: 110171-52-3.mol

Synonyms:

Chemical Property of Cyclopropanecarboxylic acid, 3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethyl-, (2-methyl[1,1'-biphenyl]-3-yl)methyl ester

Chemical Property:

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Technology Process of Cyclopropanecarboxylic acid, 3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethyl-, (2-methyl[1,1'-biphenyl]-3-yl)methyl ester

There total 4 articles about Cyclopropanecarboxylic acid, 3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethyl-, (2-methyl[1,1'-biphenyl]-3-yl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,1,1-Trichloro-2,2,2-trifluoroethane (354-58-5) + (2-methyl[1,1'-biphenyl]-3-yl)methyl cis,trans-2,2-dimethyl-3-formylcyclopropanecarboxylate (107489-30-5) + zinc (7440-66-6) → (2-methyl-3-phenylphenyl)methyl 2,2-dimethyl-3-(1-hydroxyl-2,2-dichloro-3,3,3-trifluoropropyl)cyclopropanecarboxylate (110171-52-3)

Guidance literature:

In water; N,N-dimethyl-formamide;

Reference yield: 86.0%

1,1,1-Trichloro-2,2,2-trifluoroethane (354-58-5) + (2-methyl[1,1'-biphenyl]-3-yl)methyl cis,trans-2,2-dimethyl-3-formylcyclopropanecarboxylate (107489-30-5) → (2-methyl-3-phenylphenyl)methyl (1RS,3SR)-3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethylcyclopropanecarboxylate (107686-48-6,107794-45-6,110171-52-3)

Guidance literature:

With zinc; In N,N-dimethyl-formamide;

DOI:10.1016/S0040-4039(00)84469-X

Reference yield: 35.0%

1-chloro-1,1-dibromotrifluoroethane (754-17-6) + (2-methyl[1,1'-biphenyl]-3-yl)methyl cis,trans-2,2-dimethyl-3-formylcyclopropanecarboxylate (107489-30-5) → (2-methyl-3-phenylphenyl)methyl (1RS,3SR)-3-(2,2-dichloro-3,3,3-trifluoro-1-hydroxypropyl)-2,2-dimethylcyclopropanecarboxylate (107686-48-6,107794-45-6,110171-52-3)

Guidance literature:

With zinc; In N,N-dimethyl-formamide; 1.) rt., 0.6 h, 2.) 50 deg C, 18 h;

DOI:10.1016/S0040-4039(00)84468-8

upstream raw materials:

1,1,1-Trichloro-2,2,2-trifluoroethane

(2-methyl[1,1'-biphenyl]-3-yl)methyl cis,trans-2,2-dimethyl-3-formylcyclopropanecarboxylate

1-chloro-1,1-dibromotrifluoroethane

(2-methyl-3-phenylphenyl)methyl 2,2-dimethyl-3-(2-methyl-1-propenyl)cyclopropanecarboxylate

Downstream raw materials:

(2-methyl-3-phenylphenyl)methyl (1RS,3SR)-3-(1-acetoxy-2,2-dichloro-3,3,3-trifluoropropyl)-2,2-dimethylcyclopropanecarboxylate

(2-methyl-3-phenylphenyl)methyl 2,2-dimethyl-3-(1-benzoyloxy-2,2-dichloro-3,3,3-trifluoropropyl)cyclopropanecarboxylate

(2-methyl-3-phenylphenyl)methyl 2,2-dimethyl-3-(1-tosyloxy-2,2-dichloro-3,3,3-trifluoropropyl)cyclopropanecarboxylate

(1R,3S)-3-((Z)-2-Chloro-3,3,3-trifluoro-propenyl)-2,2-dimethyl-cyclopropanecarboxylic acid 2-methyl-biphenyl-3-ylmethyl ester

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