5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE

Base Information

• Chemical Name: 5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE
• CAS No.: 110568-65-5
• Molecular Formula: C₁₀H₁₁NO
• Molecular Weight: 161.203
• Hs Code.: 2933790090
• Mol file: 110568-65-5.mol

Synonyms:5,6-Dimethylisoindolin-1-one;2,3-Dihydro-5,6-dimethyl-1H-isoindol-1-on;5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE;1H-Isoindol-1-one,2,3-dihydro-5,6-dimethyl;

Chemical Property of 5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE

Chemical Property:

• PSA: 32.59000
• LogP: 1.55720

Purity/Quality:

97% ^*data from raw suppliers

5,6-Dimethyl-2,3-dihydroisoindol-1-one ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE

There total 5 articles about 5,6-DIMETHYL-2,3-DIHYDRO-ISOINDOL-1-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4,5-dimethylphthalic anhydride (5999-20-2) → 2,3-Dihydro-5,6-dimethyl-1H-isoindol-1-on (110568-65-5)

Guidance literature:

With formamide; at 150 ℃; for 2h;

Reference yield: 72.0%

3,4-Dimethylbenzylamin (102-48-7) + carbon monoxide (201230-82-2) → 2,3-Dihydro-5,6-dimethyl-1H-isoindol-1-on (110568-65-5)

Guidance literature:

With copper (II) trifluoroacetate hydrate; 3-(trifluoromethyl)benzoic acid; palladium diacetate; In 1,2-dichloro-ethane; at 100 ℃; for 16h; under 760.051 Torr; Schlenk technique; Sealed tube;

DOI:10.1021/acs.orglett.8b00786

Reference yield: 40.0%

5,6-dimethylisoindoline-1,3-dione (20197-78-8) → 2,3-Dihydro-5,6-dimethyl-1H-isoindol-1-on (110568-65-5)

Guidance literature:

With hydrogenchloride; tin; for 5h; Heating;

upstream raw materials:

4,5-dimethylphthalic anhydride

5,6-dimethylisoindoline-1,3-dione

4,5-dimethyl-4-cyclohexene-1,2-dicarboxylic acid anhydride

2,3-dimethyl-buta-1,3-diene

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