Phosphoric trihydrazide(6CI,8CI,9CI)

Base Information

• Chemical Name: Phosphoric trihydrazide(6CI,8CI,9CI)
• CAS No.: 25841-83-2
• Molecular Formula: H9N6 O P
• Molecular Weight: 140.085
• Mol file: 25841-83-2.mol

Synonyms:

Chemical Property of Phosphoric trihydrazide(6CI,8CI,9CI)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Phosphoric trihydrazide(6CI,8CI,9CI)

There total 1 articles about Phosphoric trihydrazide(6CI,8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0) + trichlorophosphate (10025-87-3,12599-09-6,63736-95-8,39380-77-3) → hydrazine hydrochloride (2644-70-4,14011-37-1,5341-61-7) + PN6OH9 (25841-83-2)

Guidance literature:

In diethyl ether; react. of a soln. of POCl3 in ether with a suspension of anhydrous hydrazine in ether on cooling (ice-NaCl-mixt.) and stirring;; distn. of ether in vac. or high vac.; passing the aq. soln. through an anoin exchange resin (Dowex 2); evapn. in high vac.; addn. of cold ethanol at -12 °C, crystn.;;

DOI:10.1007/BF00707828

Reference yield:

PN6OH9 (25841-83-2) → Phosphate (14265-44-2,264888-19-9) + hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0)

Guidance literature:

In water; decompn. in neutral aq. soln.; formation of phosphate after a longer period of time;;

Reference yield:

PN6OH9 (25841-83-2) → hydrazine (302-01-2,78206-91-4,119775-10-9,75013-58-0)

Guidance literature:

In neat (no solvent); heating;;

upstream raw materials:

hydrazine

trichlorophosphate

Downstream raw materials:

hydrazine

Phosphate

nitrogen

silver