1H-Pyrrole-2,5-dicarboxylic acid, 3-(2-methoxy-2-oxoethyl)-4-(3-methoxy-3-oxopropyl)-, 5-(phenylmethyl) 2-(2,2,2-trichloroethyl) ester

Base Information

Chemical Name:1H-Pyrrole-2,5-dicarboxylic acid, 3-(2-methoxy-2-oxoethyl)-4-(3-methoxy-3-oxopropyl)-, 5-(phenylmethyl) 2-(2,2,2-trichloroethyl) ester
CAS No.:111807-55-7
Molecular Formula:C22H22Cl3NO8
Molecular Weight:534.778
Hs Code.:
Mol file:111807-55-7.mol

Synonyms:

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Chemical Property of 1H-Pyrrole-2,5-dicarboxylic acid, 3-(2-methoxy-2-oxoethyl)-4-(3-methoxy-3-oxopropyl)-, 5-(phenylmethyl) 2-(2,2,2-trichloroethyl) ester

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1H-Pyrrole-2,5-dicarboxylic acid, 3-(2-methoxy-2-oxoethyl)-4-(3-methoxy-3-oxopropyl)-, 5-(phenylmethyl) 2-(2,2,2-trichloroethyl) ester

There total 4 articles about 1H-Pyrrole-2,5-dicarboxylic acid, 3-(2-methoxy-2-oxoethyl)-4-(3-methoxy-3-oxopropyl)-, 5-(phenylmethyl) 2-(2,2,2-trichloroethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 115-20-8
1,1,1-trichloroethanol

: 72423-57-5
5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3methoxycarbonylmethylpyrrole-2-carboxylic acid

: 111807-55-7
2,2,2-trichloroethyl 5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrole-2-carboxylate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide;
DOI:10.1016/S0040-4039(98)00201-9

Reference yield:

: 50622-64-5
benzyl 3-(2-methoxycarbonylethyl)-4-methoxycarbonylmethyl-5-methylpyrrole-2-carboxylate

: 111807-55-7
2,2,2-trichloroethyl 5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: SO₂Cl₂ / CH₂Cl₂ / 2 h / 20 °C

2: 3.94 g / H₂O / 3 / 0.25 h / Heating

3: 85 percent / N,N'-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 15 h / 20 °C

With dmap; sulfuryl dichloride; water; dicyclohexyl-carbodiimide; 3; In dichloromethane;
DOI:10.1016/S0040-4020(01)00088-6

Reference yield:

: 77929-43-2
3-(2-Methoxycarbonyl-ethyl)-4-methoxycarbonylmethyl-5-trichloromethyl-1H-pyrrole-2-carboxylic acid benzyl ester

: 111807-55-7
2,2,2-trichloroethyl 5-benzyloxycarbonyl-4-(2-methoxycarbonylethyl)-3-methoxycarbonylmethylpyrrole-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.94 g / H₂O / 3 / 0.25 h / Heating

2: 85 percent / N,N'-dicyclohexylcarbodiimide; 4-dimethylaminopyridine / CH₂Cl₂ / 15 h / 20 °C

With dmap; water; dicyclohexyl-carbodiimide; 3; In dichloromethane;
DOI:10.1016/S0040-4020(01)00088-6