Morpholine, 4-[bis(pentachlorophenyl)acetyl]-

Base Information

Chemical Name:Morpholine, 4-[bis(pentachlorophenyl)acetyl]-
CAS No.:112312-92-2
Molecular Formula:C₁₈H₉Cl₁₀NO₂
Molecular Weight:625.805
Hs Code.:
DSSTox Substance ID:DTXSID00435191
Nikkaji Number:J482.275G
Wikidata:Q82249940

Synonyms:Morpholine, 4-[bis(pentachlorophenyl)acetyl]-;112312-92-2;DTXSID00435191;2,2-Bis(pentachlorophenyl)-1-morpholinoethanone

Suppliers and Price of Morpholine, 4-[bis(pentachlorophenyl)acetyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Morpholine, 4-[bis(pentachlorophenyl)acetyl]-

Chemical Property:

XLogP3:8.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:624.745955
Heavy Atom Count:31
Complexity:571

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COCCN1C(=O)C(C2=C(C(=C(C(=C2Cl)Cl)Cl)Cl)Cl)C3=C(C(=C(C(=C3Cl)Cl)Cl)Cl)Cl

Technology Process of Morpholine, 4-[bis(pentachlorophenyl)acetyl]-

There total 10 articles about Morpholine, 4-[bis(pentachlorophenyl)acetyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112312-91-1
isopropyl decachlorobenzilate

: 112312-92-2
bis(pentachlorophenyl)acetomorpholine

Guidance literature:: Multi-step reaction with 3 steps

1: PBr₃ / bis-(2-methoxy-ethyl) ether / Heating

2: 84 percent / H₂SO₄ / 4 h / 100 °C

3: 1) SOCl₂ / 1) 24 h, reflux, 2) toluene, RT, 1 h

With thionyl chloride; sulfuric acid; phosphorus tribromide; In diethylene glycol dimethyl ether;
DOI:10.1021/jo00042a021

Reference yield:

: 118-74-1,67471-27-6
hexachlorobenzene

: 112312-92-2
bis(pentachlorophenyl)acetomorpholine

Guidance literature:: Multi-step reaction with 4 steps

1: 1) Mg, Br(CH₂)2Br / 1) THF, 2) RT

2: PBr₃ / bis-(2-methoxy-ethyl) ether / Heating

3: 84 percent / H₂SO₄ / 4 h / 100 °C

4: 1) SOCl₂ / 1) 24 h, reflux, 2) toluene, RT, 1 h

With thionyl chloride; sulfuric acid; phosphorus tribromide; magnesium; ethylene dibromide; In diethylene glycol dimethyl ether;
DOI:10.1021/jo00042a021

Reference yield:

: 141709-01-5
ethyl decachlorobenzilate

: 112312-92-2
bis(pentachlorophenyl)acetomorpholine

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / PBr₃ / bis-(2-methoxy-ethyl) ether / Heating

2: H₂SO₄ / 120 °C

3: 1) SOCl₂ / 1) 24 h, reflux, 2) toluene, RT, 1 h

With thionyl chloride; sulfuric acid; phosphorus tribromide; In diethylene glycol dimethyl ether;
DOI:10.1021/jo00042a021