3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl ester
CAS No.:112358-09-5
Molecular Formula:C₂₈H₃₁N₃O₈
Molecular Weight:537.569
Hs Code.:

3,5-Pyridinedicarboxylic acid,
1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-,
2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl
ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl ester

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-, 2-[[(2,3-dihydro-1,4-benzodioxin-2-yl)methyl]methylamino]ethyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 119128-13-1
methyl (Z)-2-(3-nitrobenzylidene)-3-oxobutanoate

: 119747-02-3
2-amino>ethyl 3-aminocrotonate

: 112358-09-5
2-amino>ethyl methyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: In ethanol; for 2h; Heating;
DOI:10.1021/jm00126a042

Reference yield:

: 2242-31-1
2-(N-methylaminomethyl)-2,3-dihydro-1,4-benzodioxin

: 112358-09-5
2-amino>ethyl methyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: 76 percent / triethylamine / toluene / Heating

2: 70 - 80 °C

3: NH₃ / methanol / 0 °C

4: 59 percent / ethanol / 2 h / Heating

With ammonia; triethylamine; In methanol; ethanol; toluene;
DOI:10.1021/jm00126a042

Reference yield:

: 73120-83-9
N-Methyl-N-(2-hydroxyethyl)(2,3-dihydro-1,4-benzodioxin-2-yl)methanamine

: 112358-09-5
2-amino>ethyl methyl 2,6-dimethyl-4-(3-nitrophenyl)-1,4-dihydropyridine-3,5-dicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 70 - 80 °C

2: NH₃ / methanol / 0 °C

3: 59 percent / ethanol / 2 h / Heating

With ammonia; In methanol; ethanol;
DOI:10.1021/jm00126a042