Silane, [4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2 ,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)-

Base Information

Chemical Name:Silane, [4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2 ,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)-
CAS No.:112503-53-4
Molecular Formula:C₄₀H₇₄O₃Si₃
Molecular Weight:687.282
Hs Code.:

Silane,
[4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl)
dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2
,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)-

Synonyms:

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Chemical Property of Silane, [4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2 ,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)-

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Technology Process of Silane, [4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2 ,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)-

There total 5 articles about Silane, [4-[[[(1,1-dimethylethyl)dimethylsilyl]oxy]methyl]-5-[3-[[[(1,1-dimethylethyl) dimethylsilyl]oxy]methyl]-7-methyl-9-(2,6,6-trimethyl-1-cyclohexen-1-yl)-2 ,6-nonadienyl]-2-furanyl]trimethyl-, (E,E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 112503-50-1
2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

: 112503-53-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(2E,6E)-3-(tert-butyl-dimethyl-silanyloxymethyl)-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6-dienyl]-5-trimethylsilanyl-furan

Guidance literature:: Multi-step reaction with 4 steps

1: palladium dibenzylidenacetone, Ph₃P / 12 h / 50 °C

2: 2N HCl / tetrahydrofuran / 2 h / 0 °C

3: DIBAL

With hydrogenchloride; palladium dibenzylideneacetone; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95323-1

Reference yield:

: 112503-51-2
2-trimethylsilyl-4-hydroxymethyl-5-tributyl-stannylfuran

: 112503-53-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(2E,6E)-3-(tert-butyl-dimethyl-silanyloxymethyl)-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6-dienyl]-5-trimethylsilanyl-furan

Guidance literature:: Multi-step reaction with 4 steps

1: palladium dibenzylidenacetone, Ph₃P / 12 h / 50 °C

2: 2N HCl / tetrahydrofuran / 2 h / 0 °C

3: DIBAL

With hydrogenchloride; palladium dibenzylideneacetone; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95323-1

Reference yield:

: 117155-23-4
{2-[(2Z,6E)-3-Dimethoxymethyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6-dienyl]-5-trimethylsilanyl-furan-3-yl}-methanol

: 112503-53-4
3-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(2E,6E)-3-(tert-butyl-dimethyl-silanyloxymethyl)-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6-dienyl]-5-trimethylsilanyl-furan

Guidance literature:: Multi-step reaction with 3 steps

1: 2N HCl / tetrahydrofuran / 2 h / 0 °C

2: DIBAL

With hydrogenchloride; diisobutylaluminium hydride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95323-1