Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate

Base Information

Chemical Name:Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate
CAS No.:63450-00-0
Molecular Formula:C₁₈H₁₈O₄
Molecular Weight:298.339
Hs Code.:2916399090
DSSTox Substance ID:DTXSID30886591
Nikkaji Number:J429.566H
Wikidata:Q82865462
Mol file:63450-00-0.mol

Synonyms:63450-00-0;Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate;Phenol, 4,4'-(1,2-ethanediyl)bis-, 1,1'-diacetate;SCHEMBL9081470;1,2-bis(4-acetoxyphenyl)ethane;DTXSID30886591;4,4'-(1,2-Ethanediyl)bis(phenol)diacetate;Acetic acid 4-[2-(4-acetoxy-phenyl)-ethyl]-phenyl ester

Suppliers and Price of Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate

Chemical Property:

Vapor Pressure:7.28E-07mmHg at 25°C
Boiling Point:407.9°Cat760mmHg
Flash Point:200.4°C
PSA：52.60000
Density:1.155g/cm³
LogP:3.32240
XLogP3:3.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:7
Exact Mass:298.12050905
Heavy Atom Count:22
Complexity:327

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)OC1=CC=C(C=C1)CCC2=CC=C(C=C2)OC(=O)C

Technology Process of Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate

There total 5 articles about Phenol, 4,4'-(1,2-ethanediyl)bis-, diacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1657-55-2
1,2-bis(4-methoxyphenyl)ethane

: 75-36-5
acetyl chloride

: 34036-53-8
1,1'-(ethane-1,2-diylbis(6-hydroxy-3,1-phenylene))bis(ethan-1-one)

: 63450-00-0
ethane-1,2-diylbis(4,1-phenylene) diacetate

Guidance literature:: With titanium tetrachloride; In toluene; at 110 ℃;
DOI:10.1021/acsinfecdis.9b00190

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 34036-53-8
1,1'-(ethane-1,2-diylbis(6-hydroxy-3,1-phenylene))bis(ethan-1-one)

: 63450-00-0
ethane-1,2-diylbis(4,1-phenylene) diacetate

Guidance literature:: Multi-step reaction with 3 steps

1: titanium tetrachloride; zinc / tetrahydrofuran / 6 h / 80 °C

2: palladium on activated charcoal / ethanol

3: titanium tetrachloride / toluene / 110 °C

With palladium on activated charcoal; titanium tetrachloride; zinc; In tetrahydrofuran; ethanol; toluene; 1: |McMurry Reaction;
DOI:10.1021/acsinfecdis.9b00190

Reference yield:

: 4705-34-4
4,4'-dimethoxystilbene

: 34036-53-8
1,1'-(ethane-1,2-diylbis(6-hydroxy-3,1-phenylene))bis(ethan-1-one)

: 63450-00-0
ethane-1,2-diylbis(4,1-phenylene) diacetate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated charcoal / ethanol

2: titanium tetrachloride / toluene / 110 °C

With palladium on activated charcoal; titanium tetrachloride; In ethanol; toluene;
DOI:10.1021/acsinfecdis.9b00190