Technology Process of 2-Decenoic acid, 2-methyl-, ethyl ester, (E)-
There total 1 articles about 2-Decenoic acid, 2-methyl-, ethyl ester, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
morpholine; dmap; acetic acid;
In
toluene;
for 16h;
Overall yield = 50 percent; Overall yield = 53 mg; stereoselective reaction;
Reflux;
Green chemistry;
DOI:10.1021/acs.orglett.9b02291
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 96 percent / H2 / Pd black / ethyl acetate / 12 h / 760 Torr
2: 85 percent / LiAlH4 / tetrahydrofuran / 4 h / Ambient temperature
With
lithium aluminium tetrahydride; hydrogen;
palladium;
In
tetrahydrofuran; ethyl acetate;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 96 percent / H2 / Pd black / ethyl acetate / 12 h / 760 Torr
2: 85 percent / LiAlH4 / tetrahydrofuran / 4 h / Ambient temperature
3: CHCl3 / 1 h / 30 °C / Pseudomonas fluorescens lipase
4: pyridine / CCl4 / 18 h
With
pyridine; lithium aluminium tetrahydride; hydrogen;
palladium;
In
tetrahydrofuran; tetrachloromethane; chloroform; ethyl acetate;
