N-(2-Hydroxyethyl)-N-methylformamide

Base Information

• Chemical Name: N-(2-Hydroxyethyl)-N-methylformamide
• CAS No.: 1590-50-7
• Molecular Formula: C4H9 N O2
• Molecular Weight: 103.121
• Hs Code.: 2924199090
• European Community (EC) Number: 216-463-9
• UNII: L27Q94JV5G
• DSSTox Substance ID: DTXSID20166556
• Nikkaji Number: J206.830C
• Wikidata: Q83035726
• Mol file: 1590-50-7.mol

Synonyms:N-(2-Hydroxyethyl)-N-methylformamide;1590-50-7;EINECS 216-463-9;Formamide, N-(2-hydroxyethyl)-N-methyl-;L27Q94JV5G;MFCD16687622;UNII-L27Q94JV5G;SCHEMBL209008;DTXSID20166556;2-(n-formyl-n-methyl)aminoethanol;2-(N-Formyl-N-methylamino)ethanol;BAA59050;AC2477;AKOS011417023;CS-12134;SY038247;CS-0315134;A927383

Chemical Property of N-(2-Hydroxyethyl)-N-methylformamide

Chemical Property:

• Vapor Pressure: 0.000402mmHg at 25°C
• Boiling Point: 282.2°Cat760mmHg
• PKA: 14.42±0.10(Predicted)
• Flash Point: 124.5°C
• PSA: 40.54000
• Density: 1.067g/cm³
• LogP: -0.29720
• XLogP3: -0.9
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 2
• Exact Mass: 103.063328530
• Heavy Atom Count: 7
• Complexity: 55.7

Purity/Quality:

97% ^*data from raw suppliers

N-(2-Hydroxyethyl)-N-methylformamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(CCO)C=O

Technology Process of N-(2-Hydroxyethyl)-N-methylformamide

There total 3 articles about N-(2-Hydroxyethyl)-N-methylformamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + formic acid ethyl ester (109-94-4) → N-(2-hydroxyethyl)-N-methylformamide (1590-50-7)

Guidance literature:

at 20 - 60 ℃;

DOI:10.1016/j.carbpol.2009.11.001

Reference yield: 87.0%

(2-hydroxyethyl)(methyl)amine (109-83-1) + carbon dioxide (124-38-9,18923-20-1) → N-(2-hydroxyethyl)-N-methylformamide (1590-50-7)

Guidance literature:

With C₁₂H₁₄N₄*Ir⁽¹⁺⁾*C₈H₁₂*I^(1-)*C₃H₇NO; hydrogen; In methanol; at 100 ℃; for 20h; under 45004.5 Torr; Autoclave;

DOI:10.1002/asia.201800953

Reference yield:

3,4,9-triaza-2,2,9-trimethyl-1,6-dioxaspiro[4.4]non-3-ene (176964-68-4) → N-(2-hydroxyethyl)-N-methylformamide (1590-50-7)

Guidance literature:

With tert-butyl alcohol; In benzene; at 90 ℃; for 24h;

DOI:10.1139/v97-154

upstream raw materials:

(2-hydroxyethyl)(methyl)amine

formic acid ethyl ester

3,4,9-triaza-2,2,9-trimethyl-1,6-dioxaspiro[4.4]non-3-ene

carbon dioxide

Downstream raw materials:

Phthalsaeure-N-formyl-N-methylaminoethylester

N₄-benzoyl-5'-O-(4,4'-dimethoxytrityl)-3'-O-[2-(N-formyl-N-methylamino)ethoxy]-(N,N-diisopropylamino)phosphinyl-2'-deoxycytidine

N-{2-[(4-methoxybenzyl)oxy]ethyl}-N-methylformamide

Diethyl-phosphoramidous acid (2R,3S,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-(formyl-methyl-amino)-ethyl ester

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