(E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide

Base Information

Chemical Name:(E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide
CAS No.:22454-54-2
Molecular Formula:C14H10 Cl2 N2 O
Molecular Weight:293.152
Hs Code.:
NSC Number:148192
Nikkaji Number:J3.417.191B
Mol file:22454-54-2.mol

Synonyms:NSC148192;22454-54-2;NSC-148192;(E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide

Suppliers and Price of (E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.29g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:292.0170183
Heavy Atom Count:19
Complexity:319

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C(=O)NN=CC2=C(C=CC=C2Cl)Cl
Isomeric SMILES:C1=CC=C(C=C1)C(=O)N/N=C\C2=C(C=CC=C2Cl)Cl

Technology Process of (E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide

There total 5 articles about (E)-N'-(2,6-Dichlorobenzylidene)benzhydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 83-38-5
2,6-dichlorobenzaldehyde

: 613-94-5
benzoic acid hydrazide

: 22454-54-2
(E)-N'-(2,6-dichlorobenzylidene)benzohydrazide

Guidance literature:: With water; acetic acid; In neat (no solvent); at 20 ℃; for 0.133333h; stereoselective reaction; Green chemistry;
DOI:10.1039/c7gc00730b

Reference yield: 90.0%

: 83-38-5
2,6-dichlorobenzaldehyde

: 613-94-5
benzoic acid hydrazide

: 22454-54-2
2,6-Dichlorobenzylidene-benzoic-acid-hydrazide

Guidance literature:: With acetic acid; In ethanol; for 2h; Heating;

Reference yield:

: 93-89-0,99341-95-4
benzoic acid ethyl ester

: 22454-54-2
(E)-N'-(2,6-dichlorobenzylidene)benzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine / ethanol / 3 h / Heating

2: ethanol / 0.25 h / Heating

With hydrazine; In ethanol;
DOI:10.1016/0223-5234(90)90168-3