1,3-Diisopropyltriazene

Base Information

• Chemical Name: 1,3-Diisopropyltriazene
• CAS No.: 84713-95-1
• Molecular Formula: C6H15N3
• Molecular Weight: 129.205
• DSSTox Substance ID: DTXSID80233738
• Nikkaji Number: J1.366.826D
• Mol file: 84713-95-1.mol

Synonyms:1-Triazene, 1,3-bis(1-methylethyl)-;1,3-Diisopropyltriazene;84713-95-1;1,3-di(2-propyl)triazene;DTXSID80233738

Chemical Property of 1,3-Diisopropyltriazene

Chemical Property:

• Vapor Pressure: 4.59mmHg at 25°C
• Boiling Point: 146.7°Cat760mmHg
• Flash Point: 42.5°C
• Density: 0.92g/cm³
• XLogP3: 2.3
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 3
• Exact Mass: 129.126597491
• Heavy Atom Count: 9
• Complexity: 86.3

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(C)NN=NC(C)C

Technology Process of 1,3-Diisopropyltriazene

There total 6 articles about 1,3-Diisopropyltriazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2-c,3-t-diisopropyl-1-r-(H)-triaziridin → (1E)-1,3-diisopropyltriazen (84713-95-1,118644-04-5)

Guidance literature:

at 60 ℃; for 24h;

DOI:10.1002/hlca.19880710132

Reference yield: 82.0%

(1E)-1,3-diisopropyltriazen-3-carbonsaure-methylester → (1E)-1,3-diisopropyltriazen (84713-95-1,118644-04-5)

Guidance literature:

With sodium hydroxide; In methanol; for 5h; Ambient temperature;

DOI:10.1002/hlca.19880710132

Reference yield: 81.0%

pyrrolidine (123-75-1) + 2-t,3-t-diisopropyltriaziridin-1-r-carbonsaure-methylester → N-(methoxycarbonyl)pyrrolidine (56475-80-0) + (1E)-1,3-diisopropyltriazen (84713-95-1,118644-04-5) + (2E)-2,3-Diisopropyl-azimin-1-carbonsaeure-methylester (82317-28-0,82317-30-4)

Guidance literature:

In chloroform-d1; at 60 ℃; Product distribution; thermolysis;

DOI:10.1002/hlca.19880710132

upstream raw materials:

pyrrolidine

2-azidopropane

isopropylmagnesium bromide

Downstream raw materials:

isopropylamine

isopropyl alcohol