2-Azidopropane

Base Information

• Chemical Name: 2-Azidopropane
• CAS No.: 691-57-6
• Molecular Formula: C3H7N3
• Molecular Weight: 85.1087
• Hs Code.: 2929909090
• Mol file: 691-57-6.mol

Synonyms:2-Azidopropan;Isopropylazid;isopropyl azide;2-azido-propane;

Chemical Property of 2-Azidopropane

Chemical Property:

• PSA: 49.75000
• LogP: 1.15786

Purity/Quality:

98%Min ^*data from raw suppliers

2-azidopropane ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Azidopropane

There total 2 articles about 2-Azidopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl n-propylnitrosocarbamate (19935-85-4) → propan-1-ol (71-23-8) + n-propyl azide (22293-25-0) + 2-azidopropane (691-57-6) + isopropyl alcohol (67-63-0,8013-70-5)

Guidance literature:

With sodium azide; at 25 ℃; Mechanism; Product distribution; pH 8.0, 0.1 M sodium phosphate buffer;

DOI:10.1021/ja00319a027

Reference yield:

(Z)-potassium propanediazotate (87549-57-3,98114-61-5,98114-64-8) → propan-1-ol (71-23-8) + n-propyl azide (22293-25-0) + 2-azidopropane (691-57-6) + isopropyl alcohol (67-63-0,8013-70-5)

Guidance literature:

With sodium azide; potassium tert-butylate; at 25 ℃; Mechanism;

DOI:10.1021/ja00319a027

Reference yield: 95.0%

2-azidopropane (691-57-6) + prop-2-ynyl 2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside → 4-[2-acetamido-2-deoxy-4-O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-6-O-tert-butyldiphenylsilyl-β-D-glucopyranosyloxymethyl]-1-isopropyl-1H-1,2,3-triazole

Guidance literature:

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In tetrahydrofuran; water; at 20 ℃; for 12h;

DOI:10.1002/cbic.201402474

upstream raw materials:

methyl n-propylnitrosocarbamate

(Z)-potassium propanediazotate

Downstream raw materials:

di-tert-butyl nitroxide

t-butyl-t-butoxy nitroxide

4-isopropyl-5-picrylimino-1,2,3,4-thiatriazoline

(1E)-1,3-diisopropyltriazen

Refernces