Chloro(2,4,6-trimethylphenyl)germane

Base Information

Chemical Name:Chloro(2,4,6-trimethylphenyl)germane
CAS No.:114806-79-0
Molecular Formula:C₉H₁₃ClGe
Molecular Weight:229.245
Hs Code.:
DSSTox Substance ID:DTXSID10766120
Mol file:114806-79-0.mol

Synonyms:Chloro(2,4,6-trimethylphenyl)germane;114806-79-0;DTXSID10766120

Suppliers and Price of Chloro(2,4,6-trimethylphenyl)germane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Chloro(2,4,6-trimethylphenyl)germane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:0
Exact Mass:227.9761058
Heavy Atom Count:11
Complexity:115

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)[Ge]Cl)C

Technology Process of Chloro(2,4,6-trimethylphenyl)germane

There total 1 articles about Chloro(2,4,6-trimethylphenyl)germane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 128-09-6
N-chloro-succinimide

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

: 114806-79-0
(C₆H₂(CH₃)3)GeH₂Cl

Guidance literature:: In tetrahydrofuran; byproducts: succinimide; soln. of reagents in THF, N2 atm., 70°C, 3 h; evapd., pentane was added, filtered, cooled to -30°C; filtered, dried; elem. anal.;

Reference yield: 68.0%

: 592-41-6,25067-06-5
1-hexene

: 114806-79-0
(C₆H₂(CH₃)3)GeH₂Cl

: 114806-84-7
dihexylmesitylchlorogermane

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In pentane; soln. of reagents in pentane, N2 atm., 12 h, 100°C; distillation; elem. anal.;

Reference yield: 57.0%

: 114806-79-0
(C₆H₂(CH₃)3)GeH₂Cl

: 513-81-5
2,3-dimethyl-buta-1,3-diene

: 79411-69-1
C₆H₂(CH₃)3ClGeC₆H₁₀

Guidance literature:: With Bu₂Hg; In benzene; 48 h at room temperature, Hg precipitated, butadiene was added, heated at 100°C for 2 h in sealed tube; distillation, pptn. with pentane at -30°C;
DOI:10.1016/S0022-328X(00)85661-2