4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE

Base Information

Chemical Name:4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE
CAS No.:116170-97-9
Molecular Formula:C14H12N2OS2
Molecular Weight:288.38800
Hs Code.:
Mol file:116170-97-9.mol

Synonyms:4-Amino-5-benzoyl-2-ethylsulfanyl-thiophene-3-carbonitrile;

Suppliers and Price of 4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE

Chemical Property:

PSA：120.42000
LogP:4.12618

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE

There total 1 articles about 4-AMINO-5-BENZOYL-2-(ETHYLSULFANYL)-3-THIOPHENECARBONITRILE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-15-0,12122-00-8
carbon disulfide

: 75-03-6
ethyl iodide

: 70-11-1
α-bromoacetophenone

: 109-77-3
malononitrile

: 116170-97-9
3-amino-2-benzoyl-4-cyano-5-ethylthiothiophene

Guidance literature:: Yield given. Multistep reaction;
DOI:10.1016/S0040-4020(01)81450-2

Reference yield: 63.0%

: 116170-97-9
3-amino-2-benzoyl-4-cyano-5-ethylthiothiophene

: 119754-37-9
2-benzoyl-3-chloro-4-cyano-5-ethylthiothiophene

Guidance literature:: With copper dichloride; isopentyl nitrite; In acetonitrile; at 65 ℃; for 1h;
DOI:10.1016/S0040-4020(01)81450-2

Reference yield:

: 116170-97-9
3-amino-2-benzoyl-4-cyano-5-ethylthiothiophene

: 116277-19-1
2-benzoyl-3-chloro-4-cyano-5-ethylsulfinylthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / CuCl₂, isoamylnitrite / acetonitrile / 1 h / 65 °C

2: 92 percent / 83 percent 3-chloroperbenzoic acid / CH₂Cl₂ / 6 h / -5 °C

With 3-chloro-benzenecarboperoxoic acid; copper dichloride; isopentyl nitrite; In dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)81450-2