Benzoic acid, 4-[[[3,4-dihydro-3-(2-methylphenyl)-4-oxo-2-quinazolinyl]methyl]amino]-, 2-[(phenylamino)thioxomethyl]hydrazide

Base Information

Chemical Name:Benzoic acid, 4-[[[3,4-dihydro-3-(2-methylphenyl)-4-oxo-2-quinazolinyl]methyl]amino]-, 2-[(phenylamino)thioxomethyl]hydrazide
CAS No.:116285-50-8
Molecular Formula:C₃₀H₂₆N₆O₂S
Molecular Weight:534.641
Hs Code.:
Mol file:116285-50-8.mol

Synonyms:

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Chemical Property of Benzoic acid, 4-[[[3,4-dihydro-3-(2-methylphenyl)-4-oxo-2-quinazolinyl]methyl]amino]-, 2-[(phenylamino)thioxomethyl]hydrazide

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Technology Process of Benzoic acid, 4-[[[3,4-dihydro-3-(2-methylphenyl)-4-oxo-2-quinazolinyl]methyl]amino]-, 2-[(phenylamino)thioxomethyl]hydrazide

There total 4 articles about Benzoic acid, 4-[[[3,4-dihydro-3-(2-methylphenyl)-4-oxo-2-quinazolinyl]methyl]amino]-, 2-[(phenylamino)thioxomethyl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 116270-54-3
2-<(p-Hydrazinocarbonyl)phenylaminomethyl>-3-(o-tolyl)quinazolin-4(3H)-one

: 103-72-0
phenyl isothiocyanate

: 116285-50-8
N¹--N⁴-phenylthiosemicarbazide

Guidance literature:: In ethanol; for 6h; Heating;

Reference yield:

: 4-[(4-Oxo-3-o-tolyl-3,4-dihydro-quinazolin-2-ylmethyl)-amino]-benzoic acid ethyl ester

: 116285-50-8
N¹--N⁴-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / 12 h / Heating

2: 63 percent / ethanol / 6 h / Heating

With hydrazine hydrate; In ethanol;

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 116285-50-8
N¹--N⁴-phenylthiosemicarbazide

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 6 h / Heating

2: hydrazine hydrate / ethanol / 12 h / Heating

3: 63 percent / ethanol / 6 h / Heating

With pyridine; hydrazine hydrate; In ethanol;