2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide

Base Information

Chemical Name:2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide
CAS No.:116939-11-8
Molecular Formula:C9H9ClO2
Molecular Weight:184.62000
Hs Code.:2932999099
Mol file:116939-11-8.mol

Synonyms:5-Chloromethyl-2,3-dihydro-benzo[1,4]dioxine;

Suppliers and Price of 2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
5-Chloromethyl-2,3-dihydrobenzo[1,4]dioxine
50mg
$ 155.00

Crysdot
5-(Chloromethyl)-2,3-dihydrobenzo[b][1,4]dioxine 95+%
1g
$ 655.00

American Custom Chemicals Corporation
5-(CHLOROMETHYL)-2,3-DIHYDRO-1,4-BENZODIOXINE 95.00%
5G
$ 1928.08

American Custom Chemicals Corporation
5-(CHLOROMETHYL)-2,3-DIHYDRO-1,4-BENZODIOXINE 95.00%
2.5G
$ 1473.14

American Custom Chemicals Corporation
5-(CHLOROMETHYL)-2,3-DIHYDRO-1,4-BENZODIOXINE 95.00%
1G
$ 983.52

AK Scientific
5-(Chloromethyl)-2,3-dihydro-1,4-benzodioxine
1g
$ 696.00

Total 7 raw suppliers

Chemical Property of 2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide

Chemical Property:

Boiling Point:283.8±29.0 °C(Predicted)
PSA：18.46000
Density:1.264±0.06 g/cm3(Predicted)
LogP:2.19660

Purity/Quality:

97% ^*data from raw suppliers

5-Chloromethyl-2,3-dihydrobenzo[1,4]dioxine ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide

There total 4 articles about 2-AMino-N-(2,3-dihydro-benzo[1,4]dioxin-6-ylMethyl)-acetaMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 274910-19-9
(2,3-dihydrobenzo[b][1,4]dioxin-5-yl)methanol

: 116939-11-8
monochlormethylbenzo-1,4-dioxane

Guidance literature:: With thionyl chloride; In dichloromethane; at 25 ℃; for 0.25h; Neat (no solvent);

Reference yield: 45.0%

: 493-09-4
benzo-1,4-dioxane

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 116939-11-8
monochlormethylbenzo-1,4-dioxane

Guidance literature:: With hydrogenchloride; In acetic acid; at 50 ℃; for 0.333333h;
DOI:10.1007/BF00503326

Reference yield:

: 29668-43-7
2,3-dihydro-benzo[1,4]dioxine-5-carbaldehyde

: 116939-11-8
monochlormethylbenzo-1,4-dioxane

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / 1 h / 20 °C

2: pyridine; thionyl chloride / chloroform / 1 h / 20 °C

With pyridine; methanol; sodium tetrahydroborate; thionyl chloride; In chloroform;