2-Naphthalenecarbonyl azide

Base Information

• Chemical Name: 2-Naphthalenecarbonyl azide
• CAS No.: 1208-11-3
• Molecular Formula: C11H7N3O
• Molecular Weight: 197.196
• Mol file: 1208-11-3.mol

Synonyms:

Chemical Property of 2-Naphthalenecarbonyl azide

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Naphthalenecarbonyl azide

There total 1 articles about 2-Naphthalenecarbonyl azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-naphthoyl)-(4-methoxybenzoyl)methane (57114-82-6) → 2-naphthoyl azide (1208-11-3) + 4-methoxybenzoyl azide (3532-17-0)

Guidance literature:

With sodium azide; [bis(acetoxy)iodo]benzene; sodium acetate; sodium bromide; In water; acetone; at 50 ℃; for 4h;

DOI:10.1021/acs.joc.8b01417

Reference yield: 98.0%

carbon monoxide (201230-82-2) + 2-naphthoyl azide (1208-11-3) + aniline (62-53-3) → N-(phenylcarbamoyl)-2-naphthamide

Guidance literature:

With 1,10-Phenanthroline; palladium diacetate; In tetrahydrofuran; at 20 ℃; for 12h; under 15 Torr; Schlenk technique;

DOI:10.1021/acs.joc.9b01048

Reference yield: 96.0%

2-naphthoyl azide (1208-11-3) + S-methyl-S-phenylsulfoximine (4381-25-3) → C18H16N2O2S (88328-96-5,88329-04-8,88329-11-7)

Guidance literature:

With air; In acetonitrile; at 80 ℃; for 3h;

upstream raw materials:

(2-naphthoyl)-(4-methoxybenzoyl)methane

Downstream raw materials:

N-(p-nitrophenyloxycarbonyl)-β-naphthylamine