2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane

Base Information

Chemical Name:2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane
CAS No.:127693-25-8
Molecular Formula:C10H11NO4
Molecular Weight:209.202
Hs Code.:
DSSTox Substance ID:DTXSID60561283
Wikidata:Q82445014

Synonyms:2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane;127693-25-8;DTXSID60561283

Suppliers and Price of 2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:1
Exact Mass:209.06880783
Heavy Atom Count:15
Complexity:234

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C(C=CC=C1[N+](=O)[O-])C2OCCO2

Technology Process of 2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane

There total 3 articles about 2-(2-Methyl-3-nitrophenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.5%

: 23876-12-2
3-formyl-2-methyl-1-nitrobenzene

: 107-21-1
ethylene glycol

: 127693-25-8
2-(2-methyl-3-nitrophenyl)-1,3-dioxolane

Guidance literature:: boron trifluoride diethyl etherate; In chloroform; for 0.5h; Ambient temperature;
DOI:10.1002/ardp.19903230305

Reference yield:

: 23876-11-1
2-methyl-3-nitrobenzol-1-methandiol diacetate

: 127693-25-8
2-(2-methyl-3-nitrophenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: H₂O

3: 96.5 percent / BF₃*Et₂O / CHCl₃ / 0.5 h / Ambient temperature

With thionyl chloride; water; boron trifluoride diethyl etherate; In chloroform;
DOI:10.1002/ardp.19903230305

Reference yield:

: 76499-33-7
2-methyl-3-nitro-benzaldehyde dimethylacetal

: 127693-25-8
2-(2-methyl-3-nitrophenyl)-1,3-dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: H₂O

2: 96.5 percent / BF₃*Et₂O / CHCl₃ / 0.5 h / Ambient temperature

With water; boron trifluoride diethyl etherate; In chloroform;
DOI:10.1002/ardp.19903230305