methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate

Base Information

Chemical Name:methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate
CAS No.:134426-33-8
Molecular Formula:C11H11N3O4
Molecular Weight:249.22300
Hs Code.:
Mol file:134426-33-8.mol

Synonyms:methyl 2-(1-methyl-5-nitro-1H-benzodimidazol-2-yl)acetate;

Suppliers and Price of methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate

Chemical Property:

Boiling Point:447.5±25.0 °C(Predicted)
PKA:3.12±0.10(Predicted)
PSA：89.94000
Density:1.41±0.1 g/cm3(Predicted)
LogP:1.72020

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate

There total 2 articles about methyl 2-(1-methyl-5-nitro-1H-benzo[d]imidazol-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 67-56-1
methanol

: 134426-32-7
<1-Methyl-5-nitro-benzimidazolyl-(2)>acetonitril

: 134426-33-8
<1-Methyl-5-nitro-benzimidazolyl-(2)>ethansaeuremethylester

Guidance literature:: With hydrogenchloride; for 3.5h; Heating;

Reference yield:

: 41939-61-1
N₁-methyl-4-nitrobenzene-1,2-diamine

: 134426-33-8
<1-Methyl-5-nitro-benzimidazolyl-(2)>ethansaeuremethylester

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / 0.83 h / 195 - 200 °C

2: 89 percent / HCl / 3.5 h / Heating

With hydrogenchloride;

Reference yield:

: 134426-33-8
<1-Methyl-5-nitro-benzimidazolyl-(2)>ethansaeuremethylester

: 134426-36-1
<5--1-methyl-benzimidazolyl-(2)>ethansaeuremethylester

Guidance literature:: Multi-step reaction with 3 steps

1: 57 percent / H₂ / Raney-Ni / methanol / 2 h / 45 °C / 760 Torr

2: 43 percent / acetic acid; H₂O / 20 °C

3: 58 percent / SOCl₂ / CHCl₃ / 1.) overnight, 2.) 1 h, 40 deg C

With thionyl chloride; hydrogen; nickel; In methanol; chloroform; water; acetic acid;