Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]-

Base Information

• Chemical Name: Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]-
• CAS No.: 13614-61-4
• Molecular Formula: C26H20N2O
• Molecular Weight: 376.458
• DSSTox Substance ID: DTXSID20391543
• Nikkaji Number: J2.825.378H
• Mol file: 13614-61-4.mol

Synonyms:Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]-;13614-61-4;DTXSID20391543;N-Benzoyl-N,N'-diphenylbenzamidine

Chemical Property of Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]-

Chemical Property:

• XLogP3: 6.2
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 5
• Exact Mass: 376.157563266
• Heavy Atom Count: 29
• Complexity: 533

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NC2=CC=CC=C2)N(C3=CC=CC=C3)C(=O)C4=CC=CC=C4

Technology Process of Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]-

There total 15 articles about Benzamide, N-phenyl-N-[phenyl(phenylimino)methyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

N-phenyl benzoyl amide (93-98-1,5705-51-1) → N-benzoyl-N,N'-diphenylbenzamide (13614-61-4)

Guidance literature:

With 2-chloropyridine; trifluoromethylsulfonic anhydride; In dichloromethane; at -78 ℃; Reflux;

DOI:10.1016/j.tet.2009.12.034

Reference yield: 76.0%

N-phenyl-benzimidoyl chloride (4903-36-0) + C,N-diphenylnitrone (201024-81-9) → N-benzoyl-N,N'-diphenylbenzamide (13614-61-4)

Guidance literature:

With triethylamine;

Reference yield:

N,N'-dibenzoyl-N,N'-diphenyl-oxalamide (14805-58-4) → N-benzoyl-N,N'-diphenylbenzamide (13614-61-4)

Guidance literature:

at 220 - 230 ℃;

upstream raw materials:

N,N'-dibenzoyl-N,N'-diphenyl-oxalamide

ethanol

sodium ethanolate

N-phenyl-benzimidoyl chloride

Downstream raw materials:

N,N-diphenylbenzamidine

benzoic acid

N,N'-diphenylbenzamidine

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