Technology Process of Phenol, 2,4-dimethoxy-3-methyl-5-nitro-
There total 10 articles about Phenol, 2,4-dimethoxy-3-methyl-5-nitro- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol; water;
at 70 ℃;
for 1h;
DOI:10.1021/jo0522512
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 100 percent / CHCl3 / 2 h / Heating
2: 77 percent / HNO3; acetic acid; Ac2O / 1.67 h / 0 - 5 °C
3: 100 percent / HCl / H2O; methanol / 1 h / 70 °C
With
hydrogenchloride; nitric acid; acetic anhydride; acetic acid;
In
methanol; chloroform; water;
DOI:10.1021/jo0522512
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 73 percent / p-toluenesulfonic acid monohydrate; hydrogen peroxide; acetic acid / H2O / 1 h / 75 °C
2: 100 percent / CHCl3 / 2 h / Heating
3: 77 percent / HNO3; acetic acid; Ac2O / 1.67 h / 0 - 5 °C
4: 100 percent / HCl / H2O; methanol / 1 h / 70 °C
With
hydrogenchloride; dihydrogen peroxide; nitric acid; acetic anhydride; toluene-4-sulfonic acid; acetic acid;
In
methanol; chloroform; water;
DOI:10.1021/jo0522512
