Stannane, (2,3-dimethyl-2-butenyl)triphenyl-

Base Information

Chemical Name:Stannane, (2,3-dimethyl-2-butenyl)triphenyl-
CAS No.:13881-62-4
Molecular Formula:C24H26Sn
Molecular Weight:433.18
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Stannane, (2,3-dimethyl-2-butenyl)triphenyl-

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Technology Process of Stannane, (2,3-dimethyl-2-butenyl)triphenyl-

There total 3 articles about Stannane, (2,3-dimethyl-2-butenyl)triphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 639-58-7
triphenyltin chloride

: 5072-70-8
1-bromo-2,3-dimethyl-2-butene

: 13881-62-4
1-Triphenylstannyl-2,3-dimethyl-buten-⁽²⁾

Guidance literature:: With magnesium; ammonium chloride; In tetrahydrofuran; THF added to Mg and react. initiated by addn. 1,1,2-trimethylallylbromide; soln. heated to reflux and soln. of Ph3SnCl in THF and 1,1,2-trimethylallylbromide added over 2.5 h; stirred for 22 h; hydrolyzed with NH4Clsoln.; organic layer isolated, solvent removed by evapn., bis-allyls distilledoff (68-70°C at 12 torr), residue dissolved in ether, washed with MeOH-water soln. KF, ether layer dried with MgSO4, ether removed, product crystd. from hexane; elem. anal.;
DOI:10.1016/S0020-1693(00)87781-6