ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1,4-dihydropyridine-3-carboxylate

Base Information

Chemical Name:ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1,4-dihydropyridine-3-carboxylate
CAS No.:76066-86-9
Molecular Formula:C15H15NO4
Molecular Weight:273.2839
Hs Code.:

Synonyms:5-Ethoxycarbonyl-4-hydroxy-6-methyl-3-phenyl-2-pyridon;ethyl 4-hydroxy-6-methyl-3-phenyl-2-oxo-1,2-dihydropyridine-5-carboxylate;ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1H-pyridine-3-carboxylate;4-hydroxy-2-methyl-6-oxo-5-phenyl-1,6-dihydro-pyridine-3-carboxylic acid ethyl ester;ethyl 4-hydroxy-6-methyl-2-oxo-3-phenyl-1,2-dihydropyridine-5-carboxylate;

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1,4-dihydropyridine-3-carboxylate

Chemical Property:

Vapor Pressure:7.61E-09mmHg at 25°C
Boiling Point:448.9°Cat760mmHg
Flash Point:225.3°C
PSA：79.65000
Density:1.284g/cm³
LogP:2.64490

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1,4-dihydropyridine-3-carboxylate

There total 4 articles about ethyl 6-hydroxy-2-methyl-4-oxo-5-phenyl-1,4-dihydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 41867-20-3
ethyl (E)-3-aminobut-2-enoate

: 83-13-6
diethyl 2-phenylmalonate

: 76066-86-9
ethyl 4-hydroxy-6-methyl-3-phenyl-2-oxo-1,2-dihydropyridine-5-carboxylate

Guidance literature:: for 0.5h; Heating;
DOI:10.1016/0223-5234(91)90194-R

Reference yield: 57.0%

: 626-34-6
ethyl 3-aminobut-2-enoate

: 83-13-6
diethyl 2-phenylmalonate

: 76066-86-9
ethyl 4-hydroxy-6-methyl-3-phenyl-2-oxo-1,2-dihydropyridine-5-carboxylate

Guidance literature:: ethyl 3-aminobut-2-enoate; diethyl 2-phenylmalonate; at 160 ℃; for 5h;

With sodium ethanolate; In ethanol; for 2h; Heating;
DOI:10.1007/s10593-006-0070-x