[(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)

Base Information

Chemical Name:[(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)
CAS No.:105892-18-0
Molecular Formula:C10H14N2O5S
Molecular Weight:0
Hs Code.:2930909090
DSSTox Substance ID:DTXSID50909812

Synonyms:DTXSID50909812;[(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)

Suppliers and Price of [(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of [(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)

Chemical Property:

Vapor Pressure:1.05E-07mmHg at 25°C
Boiling Point:417.2°Cat760mmHg
Flash Point:206.1°C
PSA：154.67000
Density:g/cm³
LogP:1.93240
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:4
Exact Mass:274.06234272
Heavy Atom Count:18
Complexity:230

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1[N+](=O)[O-])SCC(=O)O.C(CO)N

Technology Process of [(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1)

There total 3 articles about [(4-Nitrophenyl)sulfanyl]acetic acid--2-aminoethan-1-ol (1/1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.6%

: 2002-24-6
2-amino-ethanol hydrochloride

: sodium; (4-nitro-phenylsulfanyl)-acetate

: 105892-18-0
2-hydroxyethylammonium 4-nitrophenylsulfanylacetate

Guidance literature:: sodium; (4-nitro-phenylsulfanyl)-acetate; for 1h; Reflux; Alkaline conditions;

2-amino-ethanol hydrochloride; for 2h;
DOI:10.1007/s11172-020-2742-6

Reference yield: 96.0%

: 3406-75-5
2-(4-nitrophenylthio)acetic acid

: 141-43-5
ethanolamine

: 105892-18-0
2-hydroxyethylammonium 4-nitrophenylsulfanylacetate

Guidance literature:: In ethanol; at 70 - 80 ℃; Heating;
DOI:10.1007/BF00758565

Reference yield:

: 100-00-5
4-chlorobenzonitrile

: 105892-18-0
2-hydroxyethylammonium 4-nitrophenylsulfanylacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / NaOH / H₂O / 8 h / Heating

2: 96 percent / ethanol / 70 - 80 °C / Heating

With sodium hydroxide; In ethanol; water;
DOI:10.1007/BF00758565