2,4-di-(alpha-methoxyethyl)deuteroporphyrin IX

Base Information

• Chemical Name: 2,4-di-(alpha-methoxyethyl)deuteroporphyrin IX
• CAS No.: 31444-62-9
• Molecular Formula: C36H42 N4 O6
• Molecular Weight: 626.74
• Mol file: 31444-62-9.mol

Synonyms:2,18-Porphinedipropionicacid, 7,12-bis(1-methoxyethyl)-3,8,13,17-tetramethyl- (8CI); 2,4-Di(a-methoxyethyl)deuteroporphyrin;Dimegin; Dimehin; Dimethoxyhematoporphyrin; Hematoporphyrin dimethyl ether

Chemical Property of 2,4-di-(alpha-methoxyethyl)deuteroporphyrin IX

Chemical Property:

• Boiling Point: 1085.2°Cat760mmHg
• Flash Point: 610.1°C
• PSA: 149.36000
• Density: 1.243g/cm³
• LogP: 4.36510

Purity/Quality:

98.5% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-di-(alpha-methoxyethyl)deuteroporphyrin IX

There total 6 articles about 2,4-di-(alpha-methoxyethyl)deuteroporphyrin IX which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

protoporphyrin (51589-12-9,143028-39-1,143028-40-4) → 2,4-di(α-methoxyethyl)deuteroporphyrin IX (31444-62-9)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; at 70 ℃; for 1h;

DOI:10.1007/BF00486797

Reference yield: 80.0%

methanol (67-56-1) + hematoporphyrin (14459-29-1) → 2,4-di(α-methoxyethyl)deuteroporphyrin IX (31444-62-9)

Guidance literature:

hematoporphyrin; With hydrogen bromide; acetic acid; for 4h;

methanol; at 60 ℃; for 24h;

With sodium hydroxide; In methanol; at 20 ℃;

DOI:10.1016/S0968-0896(03)00029-4

Reference yield:

hemin → 2,4-di(α-methoxyethyl)deuteroporphyrin IX (31444-62-9)

Guidance literature:

With hydrogen bromide; acetic acid; anschliessend Behandeln mit methanol.KOH;

upstream raw materials:

protoporphyrin

methanol

2,4-di(1-bromoethyl)deuteroporphyrin IX

hematoporphyrin

Downstream raw materials:

C₅₈H₆₈N₆O₁₀

C₅₈H₆₆N₄O₁₀S₂

C₆₀H₇₀N₄O₁₀